Graphite negative-electrode material with graphitization degree and hole diameter double-gradient structure, preparation method of material and application of material
A technology of graphite anode and degree of graphitization, applied in the field of production of anode materials for lithium ion batteries, can solve the problems of structure control, limited electrochemical performance of materials, lack of effective control of graphitization degree, etc., so as to improve electrical performance and optimize electrical performance. Effect
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Embodiment 1
[0076] (1) crushing, grading, and shaping the anthracite raw coal to obtain anthracite powder with a particle size range of 5-100 microns and an average particle size of 30 microns;
[0077] (2) Pretreating the anthracite powder treated in the first step. First, mix anthracite powder and potassium hydroxide as an activator in an aqueous solution at a mass ratio of 1:3, and after standing for 12 hours, continue stirring at 80° C. until the water evaporates to dryness to obtain a uniform mixture of anthracite and potassium hydroxide; The homogeneous mixture was placed in an argon atmosphere muffle furnace, and reacted at 800°C for 2 hours; after the reaction, the mixture was acid-washed and washed with water until neutral to remove excess potassium hydroxide, and activated after drying at 105°C for 24 hours After anthracite, the specific surface area is 1200m 2 / g, the average pore diameter is 5 nanometers, and the pore diameter range is 1-1000nm;
[0078] (3) After activation...
Embodiment 2
[0082] (1) crushing, grading, and shaping the anthracite raw coal to obtain anthracite powder with a particle size range of 5-100 microns and an average particle size of 30 microns;
[0083] (2) Pretreating the anthracite powder treated in the first step. First, mix anthracite powder and potassium hydroxide as an activator in an aqueous solution at a mass ratio of 1:4, and after standing for 12 hours, continue stirring at 80° C. until the water evaporates to dryness to obtain a uniform mixture of anthracite and potassium hydroxide; The homogeneous mixture was placed in an argon atmosphere muffle furnace, and reacted at 850°C for 2 hours; after the reaction, the mixture was washed with acid and water until neutral to remove excess potassium hydroxide, and was activated after drying at 105°C for 24 hours After anthracite, the specific surface area is 1500m 2 / g, the average pore diameter is 8 nanometers, and the pore diameter range is 1-1000nm;
[0084] (3) After activation, t...
Embodiment 3
[0088] (1) crushing, grading, and shaping the anthracite raw coal to obtain anthracite powder with a particle size range of 5-100 microns and an average particle size of 30 microns;
[0089] (2) Pretreating the anthracite powder treated in the first step. First, mix anthracite powder and potassium hydroxide as an activator in an aqueous solution at a mass ratio of 1:5, and after standing for 12 hours, continue stirring at 80° C. until the water evaporates to dryness to obtain a uniform mixture of anthracite and potassium hydroxide; Put the homogeneous mixture into an argon atmosphere muffle furnace, and react at 850°C for 2 hours; after the reaction, the mixture is washed with acid and water until neutral to remove excess potassium hydroxide, and dried at 105°C for 24 hours to be activated After anthracite, the specific surface area is 1800m 2 / g, the average pore diameter is 10 nanometers, and the pore diameter range is 1-1000nm;
[0090] (3) Immerse the anthracite after ac...
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