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Extreme pressure anti-wear additive and preparation method thereof

An extreme pressure anti-wear and additive technology, which is applied in the petroleum industry, lubricating compositions, etc., can solve the problems of poor water resistance, achieve good water resistance, solve the effects of easy settlement and low consumption

Inactive Publication Date: 2019-02-22
安徽中天石化股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The purpose of the present invention is to provide an extreme pressure antiwear additive with good water resistance, excellent extreme pressure and antiwear performance, and a simple and easy-to-operate preparation method, so as to solve the problem of borate antiwear in the above-mentioned background technology. Extreme pressure additives have technical problems of poor water resistance

Method used

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  • Extreme pressure anti-wear additive and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] An extreme pressure antiwear additive, comprising the following raw materials in parts by weight:

[0035] Industrial salicylic acid 10 parts, boric acid 80 parts, lithium hydroxide 3 parts, calcium hydroxide 4 parts, potassium hydroxide 40 parts, water 70 parts, base oil A 120 parts, base oil B 60 parts.

[0036] The base oil A is high-viscosity highly refined mineral oil 150BS; the base oil B is a base oil synthesized from esters.

[0037] The extreme pressure antiwear additive and its preparation method specifically comprise the following steps:

[0038] (1) Put base oil A and industrial salicylic acid into the reactor, and stir for 10-20 minutes while heating up;

[0039] (2) When the temperature is raised to 60-80° C., lithium hydroxide, calcium hydroxide and 10% water are prepared into lye and put into the reaction kettle to stir evenly with the mixture of step (1), and slowly heat up for dehydration;

[0040] (3) After the dehydration is completed, when the tem...

Embodiment 2

[0046] An extreme pressure antiwear additive, comprising the following raw materials in parts by weight:

[0047] 20 parts of industrial salicylic acid, 100 parts of boric acid, 3-4 parts of lithium hydroxide, 4-6 parts of calcium hydroxide, 60 parts of potassium hydroxide, 90 parts of water, 160 parts of base oil A, and 80 parts of base oil B.

[0048] The base oil A is high-viscosity highly refined mineral oil 150BS; the base oil B is a base oil synthesized from esters.

[0049] The extreme pressure antiwear additive and its preparation method specifically comprise the following steps:

[0050] (1) Put base oil A and industrial salicylic acid into the reactor, and stir for 10-20 minutes while heating up;

[0051] (2) When the temperature is raised to 60-80° C., lithium hydroxide, calcium hydroxide and 10% water are prepared into lye and put into the reaction kettle to stir evenly with the mixture of step (1), and slowly heat up for dehydration;

[0052] (3) After the dehydra...

Embodiment 3

[0058] An extreme pressure antiwear additive, comprising the following raw materials in parts by weight:

[0059] Industrial salicylic acid 16 parts, boric acid 90 parts, lithium hydroxide 3.5 parts, calcium hydroxide 5 parts, potassium hydroxide 50 parts, water 80 parts, base oil A 140 parts, base oil B 70 parts.

[0060] The base oil A is high-viscosity highly refined mineral oil 150BS; the base oil B is a base oil synthesized from esters.

[0061] The extreme pressure antiwear additive and its preparation method specifically comprise the following steps:

[0062] (1) Put base oil A and industrial salicylic acid into the reactor, and stir for 10-20 minutes while heating up;

[0063] (2) When the temperature is raised to 60-80° C., lithium hydroxide, calcium hydroxide and 10% water are prepared into lye and put into the reaction kettle to stir evenly with the mixture of step (1), and slowly heat up for dehydration;

[0064] (3) After the dehydration is completed, when the t...

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Abstract

The invention discloses an extreme pressure anti-wear additive. The extreme pressure anti-wear additive is prepared from the following raw materials in parts by weight: 10-20 parts of sublimed salicylic acid, 80-100 parts of boric acid, 3-4 parts of lithium hydroxide, 4-6 parts of calcium hydroxide, 40-60 parts of potassium hydroxide, 70-90 parts of water, 120-160 parts of base oil A, and 60-80 parts of base oil B. The sublimed salicylic acid and the lithium hydroxide are adopted, the calcium hydroxide is added, it is ensured that borate can be well dispersed through a special production technology, in the application process, the adverse effects on lubricant performance are minimized, the water-resisting property and the extreme pressure anti-wear property of a product are greatly improved, and the problem that the borate is prone to sedimentation is also solved effectively. The prepared extreme pressure anti-wear additive has the extremely-high extreme pressure anti-wear property andheat stability, four-ball test PB is greater than or equal to 2000 N, PD is greater than or equal to 8000 N, and the good anti-wear extreme pressure property is still be achieved when the using temperature reaches to 250 DEG C or above.

Description

technical field [0001] The invention relates to the field of petrochemical additives, in particular to an extreme pressure anti-wear additive and a preparation method thereof. Background technique [0002] About one-third of the metal materials in the world are consumed by oxidation corrosion and mechanical wear every year, and the loss in this area in my country is as high as 180 billion yuan per year. It can be seen how important it is to prevent metal corrosion and improve lubrication and anti-wear properties. For more than half a century, people have made unremitting efforts in the development of extreme pressure anti-wear and anti-friction oil agents to improve lubrication performance, and developed a variety of single agents and compound agents. Such as sulfur phosphorus (SP) gear oil extreme pressure anti-wear agent, internal combustion engine oil, anti-wear hydraulic oil zinc dialkyl dithiophosphate (ZDDP) anti-oxidation anti-corrosion anti-wear multi-effect agent, o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M173/00C10N30/06C10N30/10C10N30/12
CPCC10M173/00C10M2201/062C10M2201/087C10M2207/144C10N2030/06C10N2030/10C10N2030/12C10N2010/02C10N2010/04
Inventor 高晓谋高荣权何甲生张睿智
Owner 安徽中天石化股份有限公司
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