Preparation method of formaldehyde purifying material
A formaldehyde purification and organic solvent technology, applied in chemical instruments and methods, separation methods, other chemical processes, etc., can solve the problems of complex extraction process, complex production process, and large consumption of chemical reagents, and achieve excellent specific surface area and reduce surface area. Tension, improve the effect of interface fastness
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[0027] A preparation method of formaldehyde purification material, the specific steps of the preparation process are as follows:
[0028] a Prepare washing liquid
[0029] Mix the alcoholic organic solvent and water, stir evenly, and configure it into a washing liquid. The bath ratio of the washing liquid is 1:40~1:50, and the volume ratio of the alcohol organic solvent to water in the washing liquid is 10%:90 %~25%: 75%, stirring speed 100~250r / min, stirring time 15~30min. The alcoholic organic solvent is ethanol or isopropanol.
[0030] b Pretreatment of juncor fiber
[0031] The rush fiber is immersed in the washing liquid prepared in step a, and dried after mechanical stirring. The stirring speed is 100~250r / min, the stirring time is 15~20min, and the drying temperature is 30℃~60℃. Drying time is 20min~40min.
[0032] c Preparation of activated carbon dispersion
[0033] Place the activated carbon in a solution mixed with organic solvent and water, stir evenly and prepare activate...
Embodiment 1
[0037] According to the above process steps: mix 2mL ethanol and 18mL water, stir at 100r / min for 30min, then put 0.5g rush in the washing liquid for washing, stir at 100r / min for 30min, and dry at 30℃ for 40min to obtain washed rush , Put 0.1g 10 mesh activated carbon into 89.91g water and 9.99gN,N-dimethylacetamide mixed solution, 20℃, 100r / min stirring for 60min to obtain activated carbon dispersion, the washed rush fiber is placed on the activated carbon dispersion The activated carbon modified rush fiber is obtained by immersing in ultrasonic at 20°C and 20kHz for 1 hour and baking at 30°C for 6 hours.
Embodiment 2
[0039] According to the above process steps: mix 5mL ethanol and 15mL water, stir at 150r / min for 25min, then put 0.5g rush in the washing liquid for washing, stir at 150r / min for 25min, and bake at 40℃ for 35min to obtain washed rush , Put 10g 10 mesh activated carbon into 45g water and 45gN,N-dimethylacetamide mixture, 25℃, 200r / min stirring for 50min to obtain activated carbon dispersion, put the washed rush fiber in the activated carbon dispersion, The activated carbon modified rush fiber is obtained by immersing in 25°C, 20kHz ultrasonic for 1 hour and baking at 40°C for 5 hours.
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