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Reinforced aluminum matrix composite and preparation method thereof

A composite material and reinforced aluminum-based technology, which is applied in the field of aluminum-based composite materials, can solve the problems of particle agglomeration, weakening the reinforcement relative to the strengthening effect of aluminum-based composite materials, etc., and achieve the effect of promoting uniform distribution and overcoming segregation at grain boundaries

Inactive Publication Date: 2019-04-30
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] However, in the in-situ self-generated method, during the cooling process, the reinforcement phase particles reach the micro-nano scale, and its huge surface energy will lead to obvious particle agglomeration, which will seriously weaken the strengthening effect of the reinforcement relative to the aluminum matrix composite.

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  • Reinforced aluminum matrix composite and preparation method thereof
  • Reinforced aluminum matrix composite and preparation method thereof
  • Reinforced aluminum matrix composite and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0025] Present embodiment 1 uses ceramic TiB 2 As the reinforcement phase, the reinforcement phase reactant chooses K 2 TiF 6 and KBF 4 2024 aluminum alloy is selected as the aluminum base alloy, and the raw materials of 2024 aluminum alloy include matrix and composite elements. The matrix is ​​pure aluminum ingot with a purity of 99.95%, and the composite elements are copper, manganese, magnesium, and chromium with a purity of 99.95%. and zinc metal ingots, wherein the respective mass ratios of copper, manganese, magnesium, chromium, zinc and pure aluminum ingots are: copper: 3.8-4.9%, manganese: 0.30-1.0%, magnesium: 1.2-1.8%, chromium: 0.10% , Zinc: 0.25%, the balance is aluminum. In situ self-generated TiB in the preparation of 2024 aluminum alloy 2 The specific steps of the enhanced phase are as follows:

[0026] S1: Smelting the reinforcement phase reactants together with the raw materials of the aluminum-based alloy, so that the reinforcement phase reactants react ...

Embodiment 2

[0039] Present embodiment 2 uses intermetallic compound Mg 2 Si is used as the reinforcing phase, and aluminum-silicon alloy—Al-5Si alloy is selected as the aluminum-based alloy. The raw materials of the Al-5Si alloy include a matrix and composite elements. The matrix is ​​pure aluminum ingot with a purity of 99.95%, and the composite element is selected to have a silicon content of 30%. % Al-Si master alloy. In Situ Autogenerated Mg During Preparation of Al-5Si Alloy 2 The concrete steps of Si reinforcement phase are as follows:

[0040] S1: Smelting the reinforcement phase reactants together with the raw materials of the aluminum-based alloy, so that the reinforcement phase reactants react inside the aluminum-based composite to form a reinforced phase, forming a reinforced aluminum-based composite melt.

[0041] First, put pure aluminum, pure magnesium and aluminum-silicon intermediate alloys into a box-type resistance furnace and reserve for more than 2 hours at 200-300°C...

Embodiment 3

[0049] In Example 3, TiB 2 / Mg 2 Si as reinforcement phase, TiB 2 / Mg 2 Reactant selection for Si reinforcement phase K 2 TiF 6 and KBF 4 The mixed salt and pure magnesium with a purity of 99.95%, silicon-aluminum master alloy. Choose aluminum-silicon alloy—Al-7Si alloy as the aluminum-based alloy. The raw materials of Al-7Si alloy include matrix and compound elements. The matrix is ​​pure aluminum ingot with a purity of 99.95%, and the compound element is aluminum-silicon intermediate with a silicon content of 30%. alloy. In Situ Autogenerated TiB During Preparation of Al-7Si Alloy 2 / Mg 2 The concrete steps of Si reinforcement phase are as follows:

[0050] S1: Smelting the reinforcement phase reactants together with the raw materials of the aluminum-based alloy, so that the reinforcement phase reactants react inside the aluminum-based composite to form a reinforced phase, forming a reinforced aluminum-based composite melt.

[0051] First, according to the molar ra...

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Abstract

The invention provides a reinforced aluminum matrix composite and a preparation method thereof. The preparation method comprises the following steps that S1: the reinforced reactive materials are smelted together with raw materials of aluminum base alloy, and thus a reinforced aluminum matrix composite melting body is formed; and S2: an atomizing pressure is forced to the reinforced aluminum matrix composite melting body so that aerial fog of the reinforced aluminum matrix composite melting body can be cooled and form powder. Through gas atomization and cooling of the reinforced aluminum matrix composite melting body, the melting body forms powder in the action of the gas atomization; reinforced phase nano-particles are dispersed to be fixed in the powder without time of gathering in a high cooling rate, the high cooling rate can effectively inhibit the pushing function of the solid / liquid interface on heterogeneous particles (namely the enforced phase particles) in the solidificationprocess, and thus an in-situ self-generated enforced phase is facilitated to be uniformly distributed in an aluminum matrix composite crystal, and the problem that the reinforced phase particles segregate in a crystal boundary is overcome.

Description

technical field [0001] The invention relates to the field of aluminum-based composite materials, in particular to a reinforced aluminum-based composite material and a preparation method thereof. Background technique [0002] With the increasingly prominent energy and environmental issues, the requirements for material properties in the fields of transportation, aerospace, electronic communications, and sports industries continue to increase. The need is growing. Ceramic particle reinforced aluminum matrix composites have the advantages of plasticity and toughness of metals and high strength and high stiffness of reinforcements, and have the advantages of light weight, high specific strength, high specific modulus, and strong designability. However, traditional aluminum matrix composites have problems such as poor interfacial wettability, uneven particle distribution, and high cost, which affect their preparation and popularization and application. [0003] Reinforced alumi...

Claims

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Application Information

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IPC IPC(8): B22F9/08C22C21/18C22C32/00C22C1/10C22C21/02C22C1/03
CPCC22C1/026C22C1/03C22C1/1036C22C21/02C22C21/16C22C21/18C22C32/0005C22C32/0036C22C32/0047C22C32/0052C22C32/0073B22F9/082B22F2009/0848C22C1/1052
Inventor 蔡志勇王日初刘宇轩
Owner CENT SOUTH UNIV