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Casein-chitosan composite fiber and fabric as well as preparation methods and applications thereof

A composite fiber and composite fabric technology, applied in the direction of application, fabric, fiber chemical characteristics, etc., can solve the problems of fiber fracture and limit wide application, and achieve the effect of enhanced tensile performance, high degree of bonding, and not easy to break

Active Publication Date: 2019-05-10
SHANDONG ANQIER DECORATION ARTICLE CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] However, in the current application process of casein fiber, if the thickness of the prepared fabric is relatively thin, it is easy to cause fiber breakage in the process of stretching and breaking, which limits its wide application.

Method used

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  • Casein-chitosan composite fiber and fabric as well as preparation methods and applications thereof
  • Casein-chitosan composite fiber and fabric as well as preparation methods and applications thereof
  • Casein-chitosan composite fiber and fabric as well as preparation methods and applications thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A preparation method of casein-chitosan composite fiber, comprising the steps of: dissolving 4kg of casein in 80kg of water, adding 0.1kg of aminopropyltriethoxysilane and stirring for 30min, the stirring temperature is 50°C, adjusted by acetic acid The pH value of the system is 5.6-6.2, continue to stir for 18min, then add 1kg chitosan, 10kg water and grind for 2min, the grinding temperature is 80°C, the grinding pressure is 0.012Mpa, then add water until the water content is 80wt%, spinning to obtain a diameter of 0.01-0.06mm casein-chitosan composite fiber.

[0037] The specific steps of spinning are as follows: After spinning, it is sent to a coagulation bath for coagulation. The coagulation bath is a glutaraldehyde solution with a concentration of 0.1mol / L. The temperature of the coagulation bath is 40°C. After pre-drawing and drawing, densification The treatment was performed for 2 minutes, the densification treatment temperature was 134°C, followed by steam heat ...

Embodiment 2

[0040] A preparation method of casein-chitosan composite fiber, comprising the steps of: dissolving 10kg of casein in 30kg of water, adding 0.1kg of phenyltriethoxysilane and 0.08kg of octamethyltrisiloxane and stirring for 12min, Stirring temperature is 60°C, use acetic acid to adjust the pH value of the system to 5.6-6.2, continue to stir for 10 minutes, then add 3kg chitosan, 2kg water and grind for 10 minutes, the grinding temperature is 70°C, the grinding pressure is 0.018Mpa, and then add water to the water content The content is 70 wt%, and the casein-chitosan composite fiber with a diameter of 0.01-0.06 mm is obtained by spinning.

[0041] The specific steps of spinning are as follows: After spinning, it is sent to a coagulation bath for coagulation. The coagulation bath is a glutaraldehyde solution with a concentration of 0.18mol / L. The temperature of the coagulation bath is 20°C. After pre-drawing and drawing, densification The treatment was performed for 4 minutes, ...

Embodiment 3

[0044] A method for preparing casein-chitosan composite fiber, comprising the following steps: dissolving 5kg of casein in 75kg of water, adding 0.11kg of dimethyldichlorosilane and stirring for 28min at a stirring temperature of 51°C, using acetic acid to adjust the pH of the system The value is 5.6-6.2, continue to stir for 17 minutes, then add 1.2kg chitosan, 9kg water and grind for 3 minutes, the grinding temperature is 79 ° C, the grinding pressure is 0.013Mpa, then add water until the water content is 79wt%, spinning to obtain a diameter of 0.01 - 0.06mm casein-chitosan composite fiber.

[0045] The specific steps of spinning are as follows: After spinning, it is sent to a coagulation bath for coagulation. The coagulation bath is a glutaraldehyde solution with a concentration of 0.12mol / L. The temperature of the coagulation bath is 38°C. After pre-drawing and drawing, densification The treatment is 2.2 minutes, the densification treatment temperature is 132°C, followed b...

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Abstract

The invention discloses a casein-chitosan composite fiber and a preparation method of the casein-chitosan composite fiber. The preparation method comprises the following steps: dissolving casein intowater, adding siloxane to be stirred, regulating the pH value of a system to be 5.6-6.2, and further carrying out stirring; next, adding chitosan and water to be ground; and then, adding water, and carrying out spinning to obtain the casein-chitosan composite fiber. The invention discloses a casein-chitosan composite fabric and a preparation method thereof, the casein-chitosan composite fiber is spun to obtain yarns, and then, the yarns are woven to form a plain woven fabric. The invention discloses an application of the casein-chitosan composite fabric to underwear fabrics or wound dressings.

Description

technical field [0001] The invention relates to the technical field of textiles, in particular to a casein-chitosan composite fiber and a preparation method thereof, a casein-chitosan composite fabric and its preparation and application. Background technique [0002] The skin is the largest organ of the human body, composed of the epidermis, dermis and subcutaneous tissue. It is a natural barrier between the human body and the outside world. It plays the roles of protection, sensation, temperature regulation, secretion, excretion, absorption and immunity in the human body. The loss of water, electrolytes and acid-base balance will cause imbalance of water, electrolyte and acid-base balance, which will affect the normal absorption and metabolic balance of the human body. The skin is the first layer of barrier for the body to defend against external invasion, and it is also the largest tissue in the body. Foreign substances and microbial attack. There are many reasons for ski...

Claims

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Application Information

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IPC IPC(8): D01F8/02D01F8/18D01F1/10A41B17/00D03D15/00A61L15/32A61L15/28A61L15/42A61L15/46D03D15/292
Inventor 严春兰
Owner SHANDONG ANQIER DECORATION ARTICLE CO LTD
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