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Insecticide nanocapsule for preventing and controlling fruit tree insect pests and preparation process thereof

A nanocapsule and preparation technology, applied in the direction of insecticides, biocides, animal repellents, etc., can solve the restrictions on promotion and popularization of biological insecticides, low content of insecticidal active ingredients, and low efficiency of insecticide use High-level problems, to achieve good insecticidal control effect, improve effective utilization rate, and reduce the effect of spraying amount

Inactive Publication Date: 2019-06-04
LIANYUNGANG XIUJING LANDSCAPING ENG CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the content of insecticidal active ingredients in plants is usually low and requires a large amount of raw materials, which may cause problems in the storage and transportation of raw materials, and may also conflict with land resource utilization and environmental protection.
[0006] At present, chemical insecticides are still the main body of insecticides in the world, while some problems of biological insecticides limit their promotion and popularization
Compared with chemical pesticides, biological pesticides use natural active substances or living organisms as active ingredients, which have poorer stability and are more sensitive to external environmental factors such as temperature, humidity and light, so the storage period is shorter , the field duration is also shorter
Most of the dosage forms of biopesticides are processed by imitating chemical pesticides. Commonly used dosage forms include emulsifiable concentrates, powders, wettable powders, and suspension concentrates. Most of these traditional dosage forms are open systems, so they also have activity. Decomposition and loss of ingredients, ineffective use of pesticides

Method used

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  • Insecticide nanocapsule for preventing and controlling fruit tree insect pests and preparation process thereof
  • Insecticide nanocapsule for preventing and controlling fruit tree insect pests and preparation process thereof
  • Insecticide nanocapsule for preventing and controlling fruit tree insect pests and preparation process thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] An insecticide nanocapsule for preventing and controlling fruit tree pests, its active ingredients are spinosad and ginkgo extract, and the contents in the whole insecticide nanocapsule are 3% of spinosad and 15% of ginkgo extract %.

[0041] The preparation technology of this insecticide nanocapsule, comprises the steps:

[0042] (1) Pretreatment of plant raw materials: wash the whole ginkgo herb and place it in a blast drying oven, dry it completely at 50-60°C, then crush it with a freezer grinder, pass it through a 60-mesh sieve, and make raw material dry powder; Weigh the raw material dry powder, add it into deionized water according to the ratio of material to liquid of 1:20, and treat it with 480W microwave for 2~3min;

[0043] (2) Extraction of active ingredients: using supercritical CO 2 Extraction, weigh the pretreated ginkgo raw material dry powder, add an appropriate amount of absolute ethanol, stir evenly, add it to the extraction kettle, seal it and pass ...

Embodiment 2

[0048] Embodiment 2: the optimization experiment of preparation process

[0049] 2.1 The effect of the mass ratio of the original drug solution and the emulsifier on the encapsulation efficiency

[0050] The original drug solution and the emulsifier were mixed uniformly according to the mass ratio of 1:1, 1:2, 1:3, 1:4, 1:5, and other operations were the same as in Example 1 to prepare nanocapsules respectively and measure the encapsulation Rate. Encapsulation efficiency (%) = sum of the mass of each component of the original drug in the nanocapsule / sum of the actual input mass of the original drug × 100%.

[0051] Such as figure 1 As shown, when the mass ratio of the original drug solution to the emulsifier changed from 1:1 to 1:5, that is, when the amount of the emulsifier gradually increased, the encapsulation efficiency first increased and then decreased. When the original drug solution and the emulsifier When the volume ratio is 1:4, the encapsulation efficiency is the...

Embodiment 3

[0067] Embodiment 3: the particle size test of insecticide nanocapsule

[0068] Adopt laser particle size analyzer to carry out particle size test to the insecticide nanocapsule prepared in embodiment 1, repeat test 5 times, the result is as follows Figure 7 shown. It can be seen from the figure that the particle size of the nanocapsules is in the range of 100-300nm, and the polydispersity index PDI is in the range of 0.18-0.24, indicating that the prepared nanocapsule system has good monodispersity.

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Abstract

The invention discloses an insecticide nanocapsule for preventing and controlling insect pests of fruit trees. The insecticide nanocapsule comprises the following active components: 1-5% of spinetoramand 13-18% of a ginkgo extract. The preparation process comprises the steps of pretreatment of plant raw materials, extraction of plant components, compounding and emulsification, high-pressure homogenization, self-assembly of the nanocapsules, curing, and freeze-drying. The spinetoram and the ginkgo biloba extract are compounded, the synergistic effect is achieved, and the insecticidal activitycan be enhanced. The nano capsule obtained by the preparation process disclosed by the invention is small in particle size and high in encapsulation efficiency, not only can improve the stability of active ingredients, but also can achieve the purposes of controlling release, prolonging the lasting period and improving the effective utilization rate; therefore, the prevention and control effect onfruit tree pests is obviously improved. The insecticide nanocapsule is an ideal substitute for chemical insecticides in modern green ecological agriculture development.

Description

technical field [0001] The invention relates to the technical field of biopesticides, in particular to an insecticide nanocapsule for preventing and controlling fruit tree pests and a preparation process thereof. Background technique [0002] Agricultural products are the basic material for the survival and progress of the entire human society. However, harmful organisms such as diseases, insects, pests, and rats have been seizing and destroying the materials that human beings rely on for survival. The struggle between human beings and these harmful organisms has never ceased. Chemical pesticides are widely used because of their wide adaptability, simple operation, low cost, and remarkable effect. They have always been an important means of agricultural pest control and have made significant contributions to the high yield and income of crops. However, the long-term use of chemical pesticides has also brought various disadvantages, such as the generation of pest resistance, ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N25/28A01N65/06A01N43/22A01P7/04
Inventor 吴海燕陈海莲
Owner LIANYUNGANG XIUJING LANDSCAPING ENG CO LTD
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