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Environmentally-friendly ceramic polished brick and low-temperature preparation method thereof

A ceramic polishing brick and ceramic polishing slag technology, which is applied in the production of ceramic materials, clay products, and other household appliances, can solve the problems of low water absorption rate of mechanical strength, low utilization rate of polishing slag, and high firing temperature, and achieve social and economic goals. Significant benefits, realization of online direct resource utilization, and low firing temperature

Inactive Publication Date: 2019-06-11
SOUTH CHINA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In order to overcome the shortcomings of low utilization rate and high firing temperature of ceramic polishing slag in the prior art, the present invention adjusts the composition ratio of the liquid phase in the formula and adds a large amount of sintering aids such as feldspar and ball clay to make it burn at low temperature. A large amount of liquid phase can be generated under low temperature. Since the corrosion ability of low temperature liquid is relatively weak compared to SiC, it can control the foaming of polishing slag during firing and improve the utilization rate of ceramic polishing slag, effectively preparing ceramics with high mechanical strength and high water absorption rate. Low environmental protection polished tiles; the generation of a large number of low-temperature liquid phases can promote low-temperature sintering, reduce the sintering temperature, realize low-temperature firing of polished tiles, realize online direct resource utilization of polishing slag, and solve the problem that has long plagued the polished tile industry. The most critical technical problem to realize zero discharge of waste residue, with remarkable social and economic benefits

Method used

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  • Environmentally-friendly ceramic polished brick and low-temperature preparation method thereof
  • Environmentally-friendly ceramic polished brick and low-temperature preparation method thereof
  • Environmentally-friendly ceramic polished brick and low-temperature preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A low-temperature preparation method for environment-friendly ceramic polished tiles, comprising the following steps:

[0029] (1) After the ceramic polishing slag is sieved with an 80-mesh sieve, it is set aside;

[0030] (2) Take 25g of ceramic polishing slag, 5g of talc, 20g of potassium feldspar, 20g of black mud, 30g of kaolin, and 100ml of water, mix the raw materials by ball milling for 3 hours according to the ratio, and dry the mixed slurry in an oven. After the final powder is granulated, pass through a 60-mesh sieve to obtain the raw material powder for subsequent use;

[0031] (3) The granulated powder is subjected to dry pressing molding at a molding pressure of 20 MPa, and dried in an oven at 200° C. to obtain a polished tile green body.

[0032] (4) Put the green body into a rapid sintering furnace for sintering, the sintering temperature is 1000°C, the heating rate is 15°C / min, and the holding time is 3h.

[0033] The environment-friendly ceramic polis...

Embodiment 2

[0035] A low-temperature preparation method for environment-friendly ceramic polished tiles, comprising the following steps:

[0036] (1) After the ceramic polishing slag is sieved with an 80-mesh sieve, it is set aside;

[0037] (2) Take 10g ceramic polishing slag, 7g talc, 10g albite, 10g ball clay, 40g black mud, 23g kaolin, 110ml water, mix the raw materials according to the proportion, ball mill for 0.05h, and put the mixed slurry in the oven Dry in medium, the dried powder is granulated and passed through a 30-mesh sieve to obtain the raw material powder for later use;

[0038] (3) The granulated powder is subjected to dry pressing molding at a molding pressure of 50 MPa, and dried in an oven at 100° C. to obtain a polished tile green body.

[0039] (4) Put the green body into a rapid sintering furnace for sintering, the sintering temperature is 900°C, the heating rate is 5°C / min, and the holding time is 1h.

[0040] The environment-friendly ceramic polished tile prepa...

Embodiment 3

[0042] A low-temperature preparation method for environment-friendly ceramic polished tiles, comprising the following steps:

[0043] (1) After the ceramic polishing slag is sieved with an 80-mesh sieve, it is set aside;

[0044] (2) Take 30g of ceramic polishing slag, 5g of talc, 10g of albite, 10g of potassium feldspar, 20g of ball clay, 25g of kaolin, and 120ml of water, mix the raw materials by ball milling for 12 hours according to the ratio, and put the mixed slurry in an oven Drying in medium, the dried powder is granulated and passed through a 20-mesh sieve to obtain the raw material powder for later use;

[0045] (3) The granulated powder is subjected to dry pressing molding at a molding pressure of 60 MPa, and dried in an oven at 120° C. to obtain a polished tile green body.

[0046] (4) Put the green body into a rapid sintering furnace for sintering, the sintering temperature is 1000°C, the heating rate is 5°C / min, and the holding time is 4.5h.

[0047] The enviro...

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Abstract

The invention discloses an environmentally-friendly ceramic polished brick and a low-temperature preparation method thereof. The method comprises the following steps: performing sieving on ceramic polishing residues by using a 80-mesh sieve, mixing the sieved material and other raw materials, performing ball milling, performing granulation, and performing sieving to obtain raw material powder; performing dry-pressing forming on the raw material powder, and performing drying to obtain a polished brick green body; and performing firing on the green body under low-temperature condition of 850-1100 DEG C to obtain the ceramic polished brick, wherein the other raw materials include talc, feldspar, ball clay, black mud and kaolin, and the ceramic polishing residues account for 0.5-50% of a totalmass of the raw materials. According to the polished brick and method provided by the invention, the ceramic polished brick has a low firing temperature, firing foaming of the polishing residues canbe inhibited, the environmentally-friendly polished brick with high mechanical strength and a low water absorption rate can be prepared, the firing energy consumption of the polished brick can be greatly reduced, and industrial upgrading of polished brick companies can be promoted.

Description

technical field [0001] The invention relates to an environment-friendly ceramic polished tile and a low-temperature preparation method thereof. Background technique [0002] Ceramic polished tiles have high density, low water absorption, high mechanical strength, excellent antifouling, antifreeze and chemical stability, and occupy a large proportion in ceramic production. However, the production of polished tiles requires a polishing machine to trim, grind and polish the fired ceramics to meet the requirements of the shape, specification, size and finish of the polished tiles, thus producing a large amount of ceramic polishing slag. [0003] Since the polishing slag contains a small amount of SiC, MgO, MgCl 2 Impurities (mainly from the SiC abrasive and magnesium oxychloride binder of the polishing grinding head) and the polishing slag will cause serious foaming and deformation of the ceramics during firing when the polishing slag is directly recycled as ceramic raw materia...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B33/132C04B33/32
CPCY02P40/60
Inventor 税安泽李剑桥杜斌王聪陈为为何超罗碧云
Owner SOUTH CHINA UNIV OF TECH