A kind of preparation method and application of Lingzhu yam powder
The technology of yam powder and ling technique, applied in the field of traditional Chinese veterinary medicine, can solve the problems of incomplete extraction of biological active components, unfavorable effective absorption, waste of precious medicinal materials, etc., and achieve the effects of saving medicinal materials, low price and long duration of action.
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Embodiment 1
[0030] The preparation of embodiment 1 Lingzhu yam powder
[0031] Formulated prescription: Poria cocos 100kg, Atractylodes macrocephala 50kg, yam 25kg.
[0032] Preparation process: weigh the above-mentioned medicinal materials according to the prescription amount, pulverize them separately, pass through a 24-mesh sieve, and mix evenly.
Embodiment 2
[0033] The preparation of embodiment 2 Lingzhu yam powder
[0034] Formulated prescription: Poria cocos 5kg, Atractylodes macrocephala 45kg, yam 75kg.
[0035] Preparation Process:
[0036] (1) Take Poria cocos, Atractylodes macrocephala, and Chinese yam, put them in an extraction tank, add 750L of water to reflux and extract twice, each time for 2 hours, combine the extracts, concentrate under reduced pressure to a relative density of 1.21 (55±2°C) The thick paste was dried at 40°C and pulverized to obtain 24.4kg of water extract;
[0037] (2) For the remaining medicinal residues in step (1), add 1875L of sodium hydroxide solution with a mass fraction of 0.5%, at 30°C, stir and extract for 6 hours, centrifuge to obtain a supernatant, and adjust the supernatant with a 6mol / L hydrochloric acid solution. When the pH value of the supernatant reaches 5, slowly add 0.5 times (equivalent to the volume of the supernatant) of ethanol under stirring conditions, let it stand still, ce...
Embodiment 3
[0039] The preparation of embodiment 3 Lingzhu yam powder
[0040] Formulated prescription: Poria cocos 36kg, Atractylodes macrocephala 80kg, yam 4kg.
[0041] Preparation Process:
[0042](1) Take Poria, Atractylodes, and Yam Sanwei medicine, place the extracting tank, add 960L of water back and extract 3 times, 2.5 hours each time, merge extraction solution, concentrate to the relative density of 1.23 (55 ± 2 ℃) The thick paste was dried at 50°C and pulverized to obtain 32.8kg of water extract;
[0043] (2) For the remaining medicinal residues in step (1), add 2400L of sodium hydroxide solution with a mass fraction of 1.0%, stir and extract for 8 hours at 35°C, centrifuge to obtain a supernatant, and adjust the upper liquid with a 5mol / L hydrochloric acid solution. When the pH value of the supernatant reaches 6, slowly add 1 times the amount of ethanol (equivalent to the volume of the supernatant) under stirring conditions, let it stand still, centrifuge, take the precipit...
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