A kind of high adhesion leather finishing material and preparation method thereof
A high-adhesion, leather-based technology, applied in the field of finishing materials, can solve problems such as weak adhesion of leather
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Embodiment 1
[0044] The concrete preparation process of 3-methacrylamido dopamine (DMA) is:
[0045]A1. Take a 250mL three-neck flask, weigh 4g of sodium bicarbonate and 10g of sodium borate and dissolve them in 100mL of distilled water, blow nitrogen for half an hour to fully remove the air in the flask;
[0046] A2, take by weighing 2.5g dopamine hydrochloride and join in the above-mentioned solution, the solution presents the color of micropowder;
[0047] A3. Take another 2.5mL of methacrylic anhydride, dissolve it in 12.5ml of tetrahydrofuran (THF), and add it dropwise to the above solution after it is fully uniform. Adjust the pH value to keep the pH value above 8;
[0048] A4, blow nitrogen for half an hour, stir at room temperature for 4 hours, after the reaction is completed, transfer the resulting solution to a separatory funnel;
[0049] A5. Add 60mL ethyl acetate solution for washing, shake well, and after standing fully, take the bottom layer of powdery white solid to precip...
Embodiment 2-6
[0057] Referring to the preparation method of the high-adhesive leather finishing material provided by the present invention, according to the component contents shown in Table 1, the high-adhesive leather finishing materials of Examples 2-6 were prepared.
[0058] The high-adhesion leather finishing material raw material component content of table 1 embodiment 1-6
[0059]
[0060]
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