A blue light perovskite with high quantum yield and its preparation method and application
A perovskite and high-quantum technology, applied in chemical instruments and methods, luminescent materials, semiconductor devices, etc., can solve problems such as difficult to cover the full blue light spectrum, difficult to standard blue light emission, blue shift of the spectrum, etc., to achieve this goal Significant radiation recombination improvement, enhanced quantum yield, high quantum yield effect
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Embodiment 1
[0037] This embodiment provides a method for preparing blue light perovskite with high quantum yield. Specifically include the following steps:
[0038] 1. Prepare the precursor.
[0039] Take 0.8g Cs2 CO 3 , 40ml of octadecene and 2.5ml of oleic acid were placed in a 100ml three-necked flask, heated to 120°C for 1 hour under Ar conditions, then the solution was heated to 150°C, and kept for ten minutes to form a cesium oleate solution precursor , and then naturally cooled to room temperature for later use, and then heated to 120°C when needed.
[0040] 2. Preparation of CsPbBr 3 .
[0041] (1) Take 0.4mmol PbBr 2 and 10ml of octadecene were placed in a 100ml three-necked flask, heated to 120°C for 1 hour under Ar conditions, and then 1ml of oleic acid and 1ml of oleylamine were quickly injected, and the solution immediately became clear, and then the prepared first mixed solution Heated to 180°C for later use. In addition, in other embodiments, PbBr can also be 2 Reac...
Embodiment 2
[0059] This example is for CsPbCl 3 The luminous intensity before and after optimization was detected. Test result reference figure 2 shown by figure 2 Available, unoptimized CsPbCl 3 Low luminous intensity, optimized CsPbCl 3 Luminescence intensity is much higher than that of unoptimized CsPbCl 3 , under UV light irradiation, the optimized CsPbCl 3 The color is pink, while the optimized CsPbCl 3 The color is weaker.
Embodiment 3
[0061] This example is for CsPbCl 3 The optimized blue light spectrum and quantum yield were detected. After completing the CsPbCl 3 After optimization, the optimized CsPbCl 3 directly with CsPbBr 3 mixed to obtain CsPbBr x Cl 3-x . CbBr x Cl 3-x blue light spectrum reference image 3 As shown in a, by adjusting the CsPbCl 3 with CsPbBr 3 The ratio can achieve the coverage of the full blue light spectrum range. refer to image 3 As shown in b, when CsPbCl 3 with CsPbBr 3 When the ratio is 1:1, the quantum yield is as high as 89%, the average quantum yield is higher than 85%, and the quantum yield is much higher than that of the prior art.
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