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Preparation method for composite fireproof door core board

A technology of fire door core board and preparation steps, which is applied in the field of building materials, can solve the problems of instability, moisture-absorbing volume, and short fire-resistant limit time, and achieve the effects of inhibiting gas phase combustion, improving fire resistance, and improving fire resistance

Pending Publication Date: 2020-02-07
刘鹏
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The main technical problem to be solved by the present invention is that magnesium oxysulfide cement and magnesium oxychloride cement are used for most of the fire door core boards at present. It is short, and the fire resistance performance needs to be further improved. A preparation method for a composite fire door core board is provided.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] The thermoplastic resin is: PPE resin

[0032] Preparation of mixed products:

[0033] Take 60mL of phosphoric acid solution with a concentration of 0.4mol / L and pour it into a three-necked flask with an air duct. After heating the oil bath to 70°C, add urea into the three-necked flask, and control the molar ratio of phosphoric acid to urea to be 1:2. Continue to raise the temperature to 130°C at a heating rate of 2°C / min, add 10 g of diatomaceous earth into the three-necked flask, and keep it warm for 20 minutes to obtain a mixed product;

[0034] Preparation of magnesium fiber pulp:

[0035] Pour the above mixed product into a tray and transfer it to an oven with a set temperature of 150°C, solidify and dry for 2 hours, and then place it in a mortar and grind for 30 minutes to obtain a diatomite-based fireproof filler. Sulphate needles with a solid content of 35% Leaf pulp, magnesium oxide powder, aluminum oxide powder, and ammonia water with a mass fraction of 15% ...

Embodiment 2

[0045] The thermoplastic resin is: PI resin

[0046] Preparation of mixed products:

[0047] Take 62.5mL of phosphoric acid solution with a concentration of 0.4mol / L and pour it into a three-necked flask with an air duct, heat it in an oil bath to 75°C, then add urea into the three-necked flask, and control the molar ratio of phosphoric acid to urea to be 1:2 , continue to raise the temperature to 132.5°C at a heating rate of 2.5°C / min, add 11g of diatomaceous earth into the three-necked flask, and heat it for 25min to obtain a mixed product;

[0048] Preparation of magnesium fiber pulp:

[0049] Pour the above mixed product into a tray and transfer it to an oven with a set temperature of 175°C, solidify and dry for 2.5 hours, and then place it in a mortar and grind for 32.5 minutes to obtain a diatomite-based fireproof filler. Sulfuric acid with a solid content of 35% Salted coniferous wood pulp, magnesium oxide powder, aluminum oxide powder, and ammonia water with a mass f...

Embodiment 3

[0059] The thermoplastic resin is: PEEK resin

[0060] Preparation of mixed products:

[0061] Take 65mL of phosphoric acid solution with a concentration of 0.4mol / L and pour it into a three-necked flask with an air duct. After heating the oil bath to 80°C, add urea into the three-necked flask, and control the molar ratio of phosphoric acid to urea to be 1:2. Continue to raise the temperature to 135°C at a heating rate of 3°C / min, add 12g of diatomaceous earth into the three-necked flask, and keep it warm for 30min to obtain a mixed product;

[0062] Preparation of magnesium fiber pulp:

[0063] Pour the above mixed product into a tray and transfer it to an oven with a set temperature of 200°C, solidify and dry for 3 hours, and then place it in a mortar and grind for 35 minutes to obtain a diatomite-based fireproof filler. Sulphate needles with a solid content of 35% Leaf pulp, magnesium oxide powder, aluminum oxide powder, and ammonia water with a mass fraction of 15% are m...

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PUM

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Abstract

The invention belongs to the technical field of building materials, in particular to a preparation method for a composite fireproof door core board. According to the preparation method, after being emulsified, liquid paraffin is mixed with emulsified acrylic acid, and thermoplastic resin, the modified emulsified liquid paraffin, magnesium-containing fiber pulp, diatomite matrix fireproof filling and desulfurated gypsum powder are mixed and preheated to finally obtain the composite fireproof door core board. The diatomite matrix fireproof filling fills in wood pulp fibers, so that the binding action of magnesium salt cement and the wood pulp fibers is enhanced, and the strength of the fireproof door core board is increased; a large amount of ammonium polyphosphate fills in diatomite pores in the diatomite matrix fireproof filling, so that the fireproof performance of the fireproof door core board is improved; the liquid paraffin is emulsified with a surface active agent, so that the damp-proof performance of the fireproof door core board is enhanced; taking resin glue as dipping glue, the fireproof door core board is not liable to erode by dampness; melamine does not contain carbon,so that the fireproof performance is high; and under the micro-pore absorption action of diatomite, the liquid paraffin cannot seep from the fireproof door core board, so that the fireproof door coreboard has lasting damp-proof performance, keeps the size stability of the fireproof door core board, and has a broad application prospect.

Description

technical field [0001] The invention belongs to the technical field of building materials, and in particular relates to a preparation method of a composite fireproof door core board. Background technique [0002] The fire door is composed of skeleton, door core filling material and fireproof hardware. The filling material of the door core board is the core material of the fire door, and its quality and performance are particularly important. The filling material of the door core board traditionally uses materials such as rock wool, aluminum silicate wool, mineral wool, perlite board, foamed magnesium oxychloride cement board, and foamed cement board. Aluminum silicate wool board, rock wool, slag wool or glass wool fireproof door panels. Although these materials are light in weight and good in heat insulation, they consume a lot of energy in the production process. Pollution, it is difficult to meet environmental protection requirements, and there are problems such as poor i...

Claims

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Application Information

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IPC IPC(8): B29C67/24C08L71/12C08L79/08C08L61/16C08L91/06C08L97/02C08K13/04C08K3/22C08K7/26B29L7/00
CPCB29C67/243B29L2007/002C08K2003/222C08K2003/2227C08L61/16C08L71/123C08L79/08C08L2201/02C08L2205/03C08L2205/16C08L91/06C08L97/02C08K13/04C08K3/22C08K7/26
Inventor 刘鹏
Owner 刘鹏
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