Preparation method for composite fireproof door core board
A technology of fire door core board and preparation steps, which is applied in the field of building materials, can solve the problems of instability, moisture-absorbing volume, and short fire-resistant limit time, and achieve the effects of inhibiting gas phase combustion, improving fire resistance, and improving fire resistance
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[0030] Example 1
[0031] The thermoplastic resin is: PPE resin
[0032] Preparation of mixed products:
[0033] Take 60mL of phosphoric acid solution with a concentration of 0.4mol / L and pour it into a three-necked flask with a gas tube. After the oil bath is heated to 70°C, urea is added to the three-necked flask to control the molar ratio of phosphoric acid to urea to 1:2. Continue to heat up to 130°C at a heating rate of 2°C / min, add 10 g of diatomaceous earth to the three-necked flask, and heat it for 20 minutes to obtain a mixed product;
[0034] Preparation of magnesium fiber pulp:
[0035] Pour the above-mentioned mixed product into a tray and transfer it to an oven with a set temperature of 150℃, solidify and dry for 2h, then place it in a mortar and grind for 30min to obtain a diatomaceous earth-based fireproof filler. The sulphate needle with a solid content of 35% Leaf wood pulp, magnesium oxide powder, aluminum oxide powder, and 15% ammonia water in a mass ratio of 10:3:1...
Example Embodiment
[0044] Example 2
[0045] The thermoplastic resin is: PI resin
[0046] Preparation of mixed products:
[0047] Take 62.5mL of phosphoric acid solution with a concentration of 0.4mol / L and pour it into a three-necked flask with a gas tube. After the oil bath is heated to 75°C, add urea to the three-necked flask to control the molar ratio of phosphoric acid to urea to 1:2 , Continue to heat up to 132.5°C at a heating rate of 2.5°C / min, add 11 g of diatomaceous earth to the three-necked flask, and heat preservation for 25 minutes to obtain a mixed product;
[0048] Preparation of magnesium fiber pulp:
[0049] Pour the above-mentioned mixed product into a tray and transfer it to an oven with a set temperature of 175°C, solidify and dry for 2.5 hours, and then place it in a mortar to grind for 32.5 minutes to obtain a diatomite-based fireproof filler. The solid content of sulfuric acid is 35%. Salt coniferous wood pulp, magnesium oxide powder, aluminum oxide powder, and 15% by mass ammon...
Example Embodiment
[0058] Example 3
[0059] The thermoplastic resin is: PEEK resin
[0060] Preparation of mixed products:
[0061] Take 65mL of phosphoric acid solution with a concentration of 0.4mol / L and pour it into a three-necked flask with a gas tube. After the oil bath is heated to 80°C, add urea to the three-necked flask to control the molar ratio of phosphoric acid to urea to 1:2. Continue to heat up to 135°C at a heating rate of 3°C / min, add 12 g of diatomaceous earth to the three-necked flask, and heat preservation for 30 minutes to obtain a mixed product;
[0062] Preparation of magnesium fiber pulp:
[0063] Pour the above mixed product into a tray and transfer it to an oven with a set temperature of 200°C, solidify and dry for 3 hours, then place it in a mortar and grind for 35 minutes to obtain a diatomaceous earth-based fireproof filler. The sulfate needle with a solid content of 35% Leaf wood pulp, magnesium oxide powder, aluminum oxide powder, and 15% ammonia water in a mass ratio of ...
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