Preparation method for composite fireproof door core board
A technology of fire door core board and preparation steps, which is applied in the field of building materials, can solve the problems of instability, moisture-absorbing volume, and short fire-resistant limit time, and achieve the effects of inhibiting gas phase combustion, improving fire resistance, and improving fire resistance
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Embodiment 1
[0031] The thermoplastic resin is: PPE resin
[0032] Preparation of mixed products:
[0033] Take 60mL of phosphoric acid solution with a concentration of 0.4mol / L and pour it into a three-necked flask with an air duct. After heating the oil bath to 70°C, add urea into the three-necked flask, and control the molar ratio of phosphoric acid to urea to be 1:2. Continue to raise the temperature to 130°C at a heating rate of 2°C / min, add 10 g of diatomaceous earth into the three-necked flask, and keep it warm for 20 minutes to obtain a mixed product;
[0034] Preparation of magnesium fiber pulp:
[0035] Pour the above mixed product into a tray and transfer it to an oven with a set temperature of 150°C, solidify and dry for 2 hours, and then place it in a mortar and grind for 30 minutes to obtain a diatomite-based fireproof filler. Sulphate needles with a solid content of 35% Leaf pulp, magnesium oxide powder, aluminum oxide powder, and ammonia water with a mass fraction of 15% ...
Embodiment 2
[0045] The thermoplastic resin is: PI resin
[0046] Preparation of mixed products:
[0047] Take 62.5mL of phosphoric acid solution with a concentration of 0.4mol / L and pour it into a three-necked flask with an air duct, heat it in an oil bath to 75°C, then add urea into the three-necked flask, and control the molar ratio of phosphoric acid to urea to be 1:2 , continue to raise the temperature to 132.5°C at a heating rate of 2.5°C / min, add 11g of diatomaceous earth into the three-necked flask, and heat it for 25min to obtain a mixed product;
[0048] Preparation of magnesium fiber pulp:
[0049] Pour the above mixed product into a tray and transfer it to an oven with a set temperature of 175°C, solidify and dry for 2.5 hours, and then place it in a mortar and grind for 32.5 minutes to obtain a diatomite-based fireproof filler. Sulfuric acid with a solid content of 35% Salted coniferous wood pulp, magnesium oxide powder, aluminum oxide powder, and ammonia water with a mass f...
Embodiment 3
[0059] The thermoplastic resin is: PEEK resin
[0060] Preparation of mixed products:
[0061] Take 65mL of phosphoric acid solution with a concentration of 0.4mol / L and pour it into a three-necked flask with an air duct. After heating the oil bath to 80°C, add urea into the three-necked flask, and control the molar ratio of phosphoric acid to urea to be 1:2. Continue to raise the temperature to 135°C at a heating rate of 3°C / min, add 12g of diatomaceous earth into the three-necked flask, and keep it warm for 30min to obtain a mixed product;
[0062] Preparation of magnesium fiber pulp:
[0063] Pour the above mixed product into a tray and transfer it to an oven with a set temperature of 200°C, solidify and dry for 3 hours, and then place it in a mortar and grind for 35 minutes to obtain a diatomite-based fireproof filler. Sulphate needles with a solid content of 35% Leaf pulp, magnesium oxide powder, aluminum oxide powder, and ammonia water with a mass fraction of 15% are m...
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