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Melting and cocrystallization method of erythritol and high-power sweetening agent and product obtained by melting and cocrystallization method

A technology of high-intensity sweetener and erythritol, which is applied in the field of melt co-crystallization of erythritol and high-intensity sweetener, can solve the problem of bitterness and pungent taste, and does not involve the yield of co-crystal products and the feeling of sweetness. Not obvious and other problems, to achieve the effect of reducing production cost, low cost, and not easy to stick to the wall

Active Publication Date: 2020-02-11
BAOLINGBAO BIOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Erythritol is a natural sugar and functional sweetener. It has the advantages of low calorific value, suitable for diabetics, and anti-caries. However, its solubility at room temperature is about 37%, which is about 50% of that of sorbitol. When making high-sweet food, it is easy to crystallize out
Secondly, the sweetness of erythritol is only 70-80% of that of sucrose, and it has a cool feeling in the mouth, and the sweetness is not obvious when used alone
Sucralose and other high-intensity sweeteners are 600 times sweeter than sucrose, and also have the advantages of low calorie value similar to erythritol, suitable for diabetics, and non-cariogenic, but they have a bitter taste and acridity when used alone Waiting for bad taste
[0005] At present, there are few studies on the melt co-crystallization of erythritol and high-power sweeteners. Chinese patent document CN103262972A (application number 201310025809.5) provides a co-crystal product of erythritol and sucralose and a co-crystallization method thereof. Dissolving sucralose and adding it to the erythritol melt to obtain a co-crystallization mother solution, then cooling the co-crystallization mother solution to a certain temperature, adding seed crystals, growing crystals, and then cooling to obtain erythritol-sucralose co-crystals , but the patent does not involve the yield of co-crystal products, and the preparation process is relatively complicated

Method used

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  • Melting and cocrystallization method of erythritol and high-power sweetening agent and product obtained by melting and cocrystallization method
  • Melting and cocrystallization method of erythritol and high-power sweetening agent and product obtained by melting and cocrystallization method
  • Melting and cocrystallization method of erythritol and high-power sweetening agent and product obtained by melting and cocrystallization method

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Effect test

Embodiment 1

[0044] A method for melting co-crystallization of erythritol and high-intensity sweeteners, comprising steps as follows:

[0045] (1) Put erythritol crystals into the crystallization equipment and heat up to 148°C; after the erythritol crystals are completely dissolved, cool down to 117°C and keep warm for 30 minutes to prepare an erythritol solution;

[0046] (2) Make a suspension with high-intensity sweetener and water at a mass ratio of 1:2, then stir at 90-95°C until dissolved, then slowly add 1% of the mass of erythritol to the crystallization equipment , making erythritol-high-intensity sweetener mixed solution;

[0047] (3) Stir the erythritol-high-intensity sweetener mixture prepared in step (2) at a rate of 25°C and 300r / min for 30min, and then cool the melting and crystallization equipment to 105°C at a rate of 0.5°C / min. °C, and then rapidly cooled to 70 °C at a rate of 5 °C per minute to prepare erythritol-high-intensity sweetener co-crystals.

[0048] The high-int...

Embodiment 2

[0050] Such as figure 1 As shown, a kind of equipment of melting co-crystallization of erythritol and high power sweetener, described melting crystallization equipment comprises melting crystallization equipment main body 9, and the inner wall of described melting crystallization equipment main body 9 is provided with ordinary interlayer 3 and refrigeration interlayer 4 , the common interlayer 3 is located inside the refrigeration interlayer 4, and the inner wall surface of the common interlayer 3 is coated with a non-stick coating that does not contain fluoride and combines metals; the top of the main body 9 of the melting and crystallization equipment is provided with a feed port 1, A discharge port 2 is provided at the bottom; a cold and hot medium inlet 31, a cold and hot medium outlet 32, a refrigerant inlet 41 and a refrigerant outlet 42 are also provided on the side wall of the main body 9 of the melting and crystallization equipment;

[0051] The inside of the main bod...

Embodiment 3

[0057] A method for melting co-crystallization of erythritol and high-intensity sweeteners, comprising steps as follows:

[0058] (1) Put the erythritol crystals into the crystallization equipment and heat up to 150°C; after the erythritol crystals are completely dissolved, cool down to 118°C and keep warm for 30min to prepare the erythritol solution;

[0059] (2) Make a suspension with high-intensity sweetener and water at a mass ratio of 1:2, then stir at 90-95°C until dissolved, then slowly add 0.8% of the mass of erythritol to the crystallization equipment , making erythritol-high-intensity sweetener mixed solution;

[0060] (3) Stir the erythritol-high-intensity sweetener mixture prepared in step (2) at a rate of 28°C and 250r / min for 25min, and then cool the melting and crystallization equipment to 105°C at a rate of 0.5°C / min. °C, and then rapidly cooled to 70 °C at a rate of 5 °C per minute to prepare erythritol-high-intensity sweetener co-crystals.

[0061] The high...

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Abstract

The invention relates to a melting and cocrystallization method of erythritol and a high-power sweetening agent and a product obtained by the melting and cocrystallization method. The cocrystallization method comprises the following steps of (1) preparing an erythritol solution; (2) adding the high-power sweetening agent to the erythritol solution so as to obtain erythritol-high-power sweetening agent mixed liquor; and (3) sufficiently stirring the erythritol-high-power sweetening agent mixed liquor for 20-40min, and then quickly reducing the temperature so as to obtain an erythritol-high-power sweetening agent cocrystallization body. The erythritol-high-power sweetening agent cocrystallization body prepared by the cocrystallization method disclosed by the invention not only reserves the original nature of the erythritol being low in calorific value, resistant to decayed teeth and suitable for diabetics, but also has the advantages of being quick to dissolve, homogeneous in sugariness,long in quality guarantee period and the like; and besides, the method disclosed by the invention is simple to operate and low in cost and is suitable for large-scale industrial production.

Description

technical field [0001] The invention relates to a method for melting and co-crystallizing erythritol and a high-intensity sweetener and a product obtained, and belongs to the technical field of sugar alcohol co-crystallization. Background technique [0002] Erythritol is a natural sugar and functional sweetener. It has the advantages of low calorific value, suitable for diabetics, and anti-caries. However, its solubility at room temperature is about 37%, which is about 50% of that of sorbitol. When making high-sweet foods, it is easy to crystallize and precipitate. Secondly, the sweetness of erythritol is only 70-80% of that of sucrose, and it has a cool feeling in the mouth, and the sweetness is not obvious when used alone. Sucralose and other high-intensity sweeteners are 600 times sweeter than sucrose, and also have the advantages of low calorie value similar to erythritol, suitable for diabetics, and non-cariogenic, but they have a bitter taste and acridity when used al...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L27/30
CPCA23L27/34Y02P20/10
Inventor 李克文栾庆民孔刘娟贾慧慧熊小兰刘鎏韩敏刘浩
Owner BAOLINGBAO BIOLOGY
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