Additives for Electrolytic Capacitors and Their Applications
A technology of electrolytic capacitors and additives, applied in the direction of electrolytic capacitors, capacitors, capacitor electrolytes/absorbents, etc., can solve the problems of insufficient suppression of leakage current and leakage current, and achieve the effect of excellent withstand voltage and low leakage current
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Embodiment 1
[0213]
[0214] Into a flask equipped with a stirrer, a thermometer, and a cooling tube, 30 parts by weight of toluene [manufactured by Wako Pure Chemical Industry Co., Ltd.] and 9.5 parts by weight (132 mmol (hereinafter, referred to as mmol)) of acrylic acid [Wako Pure Chemical Co., Ltd. Pharmaceutical Industry Co., Ltd.] and 4.6 parts by weight (40 mmol) of 2-hydroxyethyl acrylate [Wako Pure Chemical Industries Co., Ltd.] were heated to 80° C. while stirring. A solution obtained by dissolving 0.9 parts by weight of azobisisobutyronitrile [manufactured by Wako Pure Chemical Industries, Ltd.] in 5 parts by weight of toluene was added dropwise there over 3 hours. After completion of the dropwise addition, in a state maintained at 80° C., it was further heated with stirring for 3 hours. Thereafter, toluene was distilled off by heating to 100° C. under a reduced pressure of 0.5 kPa, and a polymer (A-1) having a hydrophilic group was synthesized to produce an electrolytic capac...
Embodiment 2
[0215]
[0216] In Example 1, the ethylenically unsaturated monomer having a hydrophilic group was changed to a monomer described in Table 1, except that, the same procedure was carried out as in Example 1 to prepare a polymer containing a hydrophilic group ( A-2) The additive (P-2) for electrolytic capacitors. The Mn of the polymer (A-2) was 5,300, and the Tg was 11°C.
Embodiment 3
[0217]
[0218] In Example 1, the ethylenically unsaturated monomer having a hydrophilic group was changed to a monomer described in Table 1, except that, the same procedure was carried out as in Example 1 to prepare a polymer containing a hydrophilic group ( A-3) Additive (P-3) for electrolytic capacitors. The Mn of the polymer (A-3) was 5,500, and the Tg was 4°C.
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