Method for preparing gold electrolyte through gold electrolysis anode mud
An anode slime and electrolyte technology, which is applied in the electrolysis process, electrolysis components, photography process, etc., can solve problems such as increasing capital occupation, and achieve the effect of reducing volatilization loss, reducing the amount of raw materials, and reducing the risk of introducing impurity carbon.
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[0057] Example 1
[0058] Use gold electrolysis anode slime to prepare gold electrolyte according to the following method:
[0059] (1) Aqua regia dissolution: Take 0.747kg of anode bag containing gold electrolytic anode slime (including 0.526kg of gold electrolytic anode slime) and place it in a crucible, first add 1.5L concentrated hydrochloric acid, then add 0.5L concentrated nitric acid, and heat to 50 Keep stirring until the anode mud is completely dissolved to obtain a red gold solution; take out, wash and dry the anode bag for subsequent use. The obtained gold solution was filtered to obtain filtrate and insoluble matter. Collect the insoluble matter and recover the precious metals after a certain amount.
[0060] (2) Hydrogen peroxide concentration and nitrate removal: The filtrate obtained in step (1) is heated to a boiling state, and hydrogen peroxide is added in batches to remove nitrate. Continue stirring during the nitrate removal process until no yellow smoke is gener...
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[0064] Example 2
[0065] Use gold electrolysis anode slime to prepare gold electrolyte according to the following method:
[0066] (1) Aqua regia dissolution: Take 1.628kg of anode bag containing gold electrolytic anode slime (including gold electrolytic anode slime 1.204kg) and place it in a crucible, first add 3L concentrated hydrochloric acid, then add 1L concentrated nitric acid, heat to 60℃ and Continue to stir until the anode mud is completely dissolved to obtain a red gold solution; take out, wash and dry the anode bag for subsequent use. The solution was filtered to obtain filtrate and insoluble matter. Collect the insoluble matter and recover the precious metals after a certain amount.
[0067] (2) Hydrogen peroxide concentration and nitrate removal: The filtrate obtained in step (1) is heated to boiling, and hydrogen peroxide is added in batches to remove nitrate. The stirring is continued during the nitrate removal process until no yellow smoke is generated after the ad...
Example Embodiment
[0071] Example 3
[0072] Use gold electrolysis anode slime to prepare gold electrolyte according to the following method:
[0073] (1) Aqua regia dissolution: Take 2.365kg of anode bag containing gold electrolytic anode mud (including gold electrolytic anode mud 1.701kg) and place it in a crucible, first add 4.5L of concentrated hydrochloric acid, then add 1.5L of concentrated nitric acid, and heat to 70 Keep stirring until the anode mud is completely dissolved to obtain a red gold solution; take out, wash and dry the anode bag for subsequent use. The solution was filtered to obtain filtrate and insoluble matter. Collect the insoluble matter and recover the precious metals after a certain amount.
[0074] (2) Hydrogen peroxide concentration and nitrate removal: The filtrate obtained in step (1) is heated to boiling, and hydrogen peroxide is added in batches to remove nitrate. The stirring is continued during the nitrate removal process until no yellow smoke is generated after the ...
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