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Antistatic smokeless sulfur-free firecracker nitrate agent and preparation method thereof

A technology of antistatic agent and firecracker nitrate, applied in explosives processing equipment, nitrated acyclic/alicyclic/heterocyclic amine explosive composition, explosives, etc., can solve problems such as smoke pollution, improve mechanical properties, and make raw materials easy to use The effect of simple process

Pending Publication Date: 2020-04-10
江西吉润花炮新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The present invention provides an antistatic smokeless and sulfur-free firecracker nitrate and its preparation method in order to solve the smoke pollution problem existing after the firecracker nitrate is set off.

Method used

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  • Antistatic smokeless sulfur-free firecracker nitrate agent and preparation method thereof
  • Antistatic smokeless sulfur-free firecracker nitrate agent and preparation method thereof
  • Antistatic smokeless sulfur-free firecracker nitrate agent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] An antistatic smokeless and sulfur-free firecracker nitrate agent, the mass percentage of each component is as follows:

[0028]

[0029] Take 55.62g of nitrobamboo cellulose powder and divide it into two groups, A and B, wherein 15.62g of group A and 40g of group B, and dissolve the nitrobamboo cellulose powder of group A in 156.2g of ethyl acetate, and stir under ultrasonic dispersion conditions After 2.5 hours, continue to stir, add 2.72g of dicyandiamide, 10.47g of 1,3-dimethyl-1,3-diphenylurea and 16.80g of magnesium stearate, and stir evenly to obtain bamboo nitrate Cellulose mixed sol;

[0030] Add 1.91g of α-hydroxyethylamine phosphate to 19.1g of acetone, stir for 70 minutes in an ultrasonic state, and then put it into a spray gun to prepare an antistatic agent spray;

[0031] In the state of stirring and ultrasonic dispersion, add 123.74g of passivated hexogen, 21.90g of modified ammonium dinitramide and group B nitrobamboo cellulose into the nitrocellulos...

Embodiment 2

[0036] An antistatic smokeless and sulfur-free firecracker nitrate agent, the mass percentage of each component is as follows:

[0037]

[0038]

[0039] Take 11.12kg of nitrobamboo cellulose powder and divide it into two groups, A and B, wherein 2.12kg of group A and 9kg of group B, and dissolve the nitrobamboo cellulose powder of group A in 21.2kg of ethyl acetate, and stir under the condition of ultrasonic dispersion 3 hours, then continue to stir, add 0.76kg of dicyandiamide, 1.38kg of 1,3-dimethyl-1,3-diphenylurea and 3.68kg of magnesium stearate, stir evenly, and obtain bamboo nitrate Cellulose mixed sol;

[0040]0.78kg of stearamidopropyl hydroxyethyl quaternary ammonium nitrate isopropyl was added to 7.8kg of acetone, stirred for 80 minutes in an ultrasonic state, and then packed into a spray gun to obtain an antistatic agent spray liquid;

[0041] In the state of stirring and ultrasonic dispersion, add 40.82kg of passivated hexogen, 4.62kg of modified ammonium ...

Embodiment 3

[0046] An antistatic smokeless and sulfur-free firecracker nitrate agent, the mass percentage of each component is as follows:

[0047]

[0048] Take 23.73kg of nitrobamboo cellulose powder and divide it into two groups, A and B, wherein group A is 8.73kg and group B is 15kg. Dissolve the nitrobamboo cellulose powder in group A in 87.3kg of ethyl acetate and stir under ultrasonic dispersion conditions 3 hours, then continue to stir, add 2.59kg of dicyandiamide, 3.62kg of 1,3-dimethyl-1,3-diphenylurea and 7.12kg of magnesium stearate, and stir evenly to obtain bamboo nitrate Cellulose mixed sol;

[0049] 1.70 kg of alkyl dicarboxymethyl betaine was added to 17 kg of acetone, stirred for 90 minutes in an ultrasonic state, and then loaded into a spray gun to obtain an antistatic agent spray liquid;

[0050] In the state of stirring and ultrasonic dispersion, add 62.18kg of passivated hexogen, 9.44kg of modified ammonium dinitramide and group B nitrobamboo cellulose into the n...

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Abstract

The invention relates to an antistatic smokeless sulfur-free firecracker nitrate agent and a preparation method thereof, belonging to the field of environment-friendly pyrotechnic compositions. The firecracker nitrate agent comprises, desensitized hexogen, nitrified bamboo cellulose, modified ammonium dinitramide, magnesium stearate, 1,3-dimethyl-1,3-diphenyl urea, dicyandiamide, amino silicon oiland an antistatic agent. According to the invention, desensitized hexogen is used as a main component, and modified ammonium dinitramide is used as an oxidant, so an oxygen content is sufficient, andcombustion effect is ensured; the nitrified bamboo cellulose, 1,3-dimethyl-1,3-diphenyl urea, magnesium stearate and dicyandiamide are adopted, and the antistatic agent and amino silicone oil are added, so the mechanical properties, stability and antistatic capacity of the firecracker nitrate agent can be remarkably improved, and the safety and reliability of the firecracker nitrate agent in theprocesses of production, storage and use are guaranteed; meanwhile, the firecracker nitrate agent does not contain a sulfur element or any metal powder, so the preparation of the smokeless sulfur-freefirecracker nitrate agent can be truly realized.

Description

technical field [0001] The invention relates to an antistatic smokeless and sulfur-free firecracker nitrate agent and a preparation method thereof, belonging to the field of environment-friendly pyrotechnic agents. Background technique [0002] Fireworks and firecrackers have been widely used in Chinese festivals and have been popular for a long time, and the setting off of firecrackers has a history of nearly 1,000 years. In recent years, due to the continuous growth of consumption, the lack of environmental protection awareness and the surge of manufacturers, the discharge of fireworks and firecrackers has caused serious environmental pollution and serious harm to human health. [0003] The main ingredients of today's pyrotechnics are potassium nitrate, sulfur and charcoal, some also contain potassium chlorate, and even metal powder is added. Although carbon powder and metal powder can improve the antistatic ability of pyrotechnics, the discharge of finished fireworks and...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C06B25/34C06B21/00
CPCC06B21/0066C06B25/34
Inventor 刘吉平李琪军刘克普吉伟生于保藏周天驰
Owner 江西吉润花炮新材料科技有限公司
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