A kind of preparation method and application of bamboo-based biochar phosphorus removal adsorbent
A phosphorus adsorbent, biochar technology, applied in chemical instruments and methods, adsorbed water/sewage treatment, water pollutants, etc., can solve the problems of poor selectivity, low adsorption capacity, limited economic value, etc., to reduce the preparation cost, The effect of high saturated adsorption capacity and high removal rate
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Embodiment 1
[0041] The preparation method of present embodiment bamboo-based biochar dephosphorization adsorbent comprises the following steps:
[0042] Bamboo is crushed into bamboo chips with a particle size of ≤1.5 mm, and 10 g of bamboo chips are added to 0.3 mol / L (acetic acid) in 2 L of acetic acid-ethanol-water solution (the volume ratio of ethanol to water is 3:1) and mechanically stirred for 5 hours, then washed Filter and dry at 100°C. Mix the dried bamboo chips with 10L of clean seawater and stir for 10h. Then wash and filter with water until the filtrate is detected by silver nitrate and does not produce white precipitate, that is, there is no chloride ion in the filtrate, indicating that the sample is washed clean, and then dried at 160 ° C, and finally in argon atmosphere and 850 ° C tube type Calcined in a furnace for 30 minutes to obtain a modified bamboo-based biochar phosphorus removal adsorbent, marked as ZS850.
Embodiment 2
[0044] The difference between this example and Example 1 is that the calcination temperature of Example 2 is 650° C., and the others are the same as Example 1. The obtained modified bamboo-based biochar dephosphorization adsorbent is marked as ZS650.
Embodiment 3
[0046] The difference between this example and Example 1 is that the calcination temperature of Example 3 is 750° C., and the others are the same as Example 1. The obtained modified bamboo-based biochar dephosphorization adsorbent is marked as ZS750.
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