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Preparation method and equipment of SiC fiber prepreg tape with attached interface layer

A technology of interface layer and prepreg tape, which is applied in fiber processing, equipment configuration for processing textile materials, liquid/gas/steam fiber/sliver/roving processing, etc. It can solve the problems of low elongation at break and small elasticity, etc. Achieve excellent adhesion performance, consistent performance, and reduce surface damage

Active Publication Date: 2020-04-24
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But prior art mainly researches on carbon fiber prepreg, as the patent No. CN103158209B discloses the preparation method of continuous carbon fiber reinforced thermoplastic prepreg, the patent No. CN 106239937 A discloses the preparation of continuous fiber reinforced thermoplastic prepreg Belt device, considering that silicon carbide fiber is a brittle material with low elongation at break and low elasticity, there is an urgent need for a preparation method and equipment for preparing silicon carbide fiber prepreg tape to improve the performance of silicon carbide fiber composite materials

Method used

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  • Preparation method and equipment of SiC fiber prepreg tape with attached interface layer
  • Preparation method and equipment of SiC fiber prepreg tape with attached interface layer
  • Preparation method and equipment of SiC fiber prepreg tape with attached interface layer

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0050] This embodiment provides a method for preparing a SiC fiber prepreg tape with an interface layer attached, comprising the following steps:

[0051] S1: After the continuous silicon carbide fiber bundle is unrolled, it is introduced to the tension wheel 4 through the godet roller 1 and the guide wheel 2, and the tension of the tension wheel 4 is 1N, which is used to stabilize the tension of the continuous silicon carbide fiber bundle;

[0052] S2: The tension wheel sends the continuous silicon carbide fiber bundle straight into the desizing device, and the processing solvent is acetone, so that the sizing agent on the surface of the continuous silicon carbide fiber is fully dissolved, and the continuous silicon carbide fiber bundle is unfolded;

[0053] S3: The continuous silicon carbide fiber bundle after desizing treatment is introduced into the gluing device through the guide wheel, and through the traction of the active rubber wheel in the gluing device and the lubric...

Embodiment 2

[0075] Compared with Example 1, the preparation method and equipment of the SiC fiber prepreg tape with interface layer attached in this embodiment differ in that:

[0076] The tension adjusted by the tension wheel 4 is 5N.

[0077] The heat treatment temperature is 60° C., and the solvent is absolute ethanol.

[0078] The glue in the gluing device is phenolic resin, the heating temperature is controlled at 80°C, and the thickness of the resin is controlled at 0.3mm.

[0079] The number of said rollers 9 is 30, and the heating temperature of said rollers is controlled at 160°C.

[0080] The diameter of described wind-up roll 10 is 320mm, and rotational speed is 4r / min, and the pitch of described rolling roll 10 is 2mm, and the thickness that obtains prepreg tape is 0.2mm, and width is 1000mm.

[0081] The thickness gauge 13 is a laser thickness gauge.

Embodiment 3

[0083] Compared with Example 1, the preparation method and equipment of the SiC fiber prepreg tape with interface layer attached in this embodiment differ in that:

[0084] The tension adjusted by the tension wheel 4 is 10N.

[0085] The heat treatment temperature of the desizing device is 80° C., and the solvent is absolute ethanol.

[0086] The glue in the gluing device is phenolic resin, the heating temperature is controlled at 100°C, and the thickness of the resin is controlled at 0.1mm.

[0087] The number of the roller rollers 9 is 20, and the heating temperature of the roller rollers is controlled at 100°C.

[0088] The diameter of the winding roll 10 is 300mm, the rotational speed is 5r / min, and the pitch of the rolling roll 11 is 1.6mm, the thickness of the obtained prepreg tape is 0.1mm, and the width is 500mm.

[0089] The thickness gauge 13 is an ultrasonic thickness gauge.

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Abstract

The invention provides a preparation method of a SiC fiber prepreg tape with an attached interface layer. The preparation method comprises the following steps of introducing a continuous silicon carbide fiber bundle onto a tension pulley after being unwound through a godet roller and a guide wheel, sending the continuous silicon carbide fiber bundle straightly into a desizing device to expand thecontinuous silicon carbide fiber bundle; introducing the continuous silicon carbide fiber bundle onto a gluing device, so that glue fully infiltrates the continuous silicon carbide fiber, after that,introducing the continuous silicon carbide fiber bundle to a silk spreading device, and fully spreading and sizing the continuous silicon carbide fiber bundle by a drawing-in roller in the silk spreading device; and enabling the fully spread and sized continuous silicon carbide fiber bundle to enter a winding roller to obtain the flat and uniform prepreg tape. The prepreg tape prepared by the invention not only can greatly improve the toughness of the silicon carbide fiber, but also a deposited interface layer is uniform, meanwhile, the overlapped parts of two adjacent fiber bundles in the prepreg tape are few, the fiber bundle is good in flatness and thin in thickness, in addition, the preparation equipment can control parameters in real time, and full automation and complete controllability can be realized.

Description

technical field [0001] The invention relates to the technical field of prepreg preparation, in particular to a method and equipment for preparing a SiC fiber prepreg with an interface layer. Background technique [0002] With the continuous advancement of aerospace and aviation technology, the requirements for materials are getting higher and higher. Compared with various alloys, composite materials made of carbon fiber or silicon carbide fiber have better density, high temperature resistance and service life. There are obvious advantages, among which, the ceramic matrix composite material prepared by silicon carbide fiber has more outstanding advantages in high temperature oxidation resistance. [0003] The existing traditional method of preparing silicon carbide fiber ceramics is to weave first and then deposit the interface layer. For example, the patent with the publication number CN109650924A adopts the method of polar weaving the prefabricated body first and then depos...

Claims

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Application Information

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IPC IPC(8): D04H1/4242D04H1/587D04H1/655D06B3/02D06B23/20D06B23/02D06B23/04D06B23/22D06B23/14D06M15/41
CPCD04H1/4242D04H1/587D04H1/655D06B3/02D06B23/02D06B23/023D06B23/04D06B23/14D06B23/20D06B23/22D06M15/41
Inventor 阳海棠王培生黄小忠
Owner CENT SOUTH UNIV
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