Preparation method of carbon quantum dot modified n-n type MFe12O19/CeO2 magnetic separation photocatalyst
A technology of mfe12o19 and carbon quantum dots, which is applied in the direction of metal/metal oxide/metal hydroxide catalysts, physical/chemical process catalysts, chemical instruments and methods, etc., can solve the problems of poor photocatalytic degradation ability and achieve cheap raw materials , Excellent effect, various effects
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Embodiment 1
[0024]A carbon quantum dot modified n-n type MFe 12 o 19 / CeO 2 The preparation method of magnetic separation photocatalyst comprises the following steps:
[0025] Step 1: Weigh 50g of glucose and dissolve it in 80mL of aqueous solution. After it is completely dissolved, transfer it to a reaction kettle lined with polytetrafluoroethylene, and place the reaction kettle in a drying oven at a constant temperature of 180°C for 5 hours , to obtain water-soluble carbon quantum dots.
[0026] Step 2: Press SrFe 12 o 19 The mol ratio of Sr and Fe in the middle is that the ratio of Sr:Fe=1:12 takes by weighing soluble 0.2442g strontium nitrate, soluble 5.5938g ferric nitrate, takes by weighing and cation molar ratio is the chelating agent citric acid 4.7282g of 1.5:1; Weigh 20g of gel-collapsing agent glucose; weigh 9.5958g of acrylamide with a molar ratio of 9:1 to the cation; weigh 1.9192g of a cross-linking agent methylenebisacrylamide with a mass ratio of 5:1 to acrylamide Sl...
Embodiment 2
[0030] A carbon quantum dot modified n-n type MFe 12 o 19 / CeO 2 The preparation method of magnetic separation photocatalyst comprises the following steps:
[0031] Step 1: Weigh 50g of glucose and dissolve it in 80mL of aqueous solution. After it is completely dissolved, transfer it to a reaction kettle lined with polytetrafluoroethylene, and place the reaction kettle in a drying oven at a constant temperature of 180°C for 5 hours , to obtain water-soluble carbon quantum dots.
[0032] Step 2: Press SrFe 12 o 19 The mol ratio of Sr and Fe in the middle is that the ratio of Sr:Fe=1:12 takes by weighing soluble 0.2442g strontium nitrate, soluble 5.5938g ferric nitrate, takes by weighing and cation molar ratio is the chelating agent citric acid 4.7282g of 1.5:1; Weigh 20g of gel-collapsing agent glucose; weigh 9.5958g of acrylamide with a molar ratio of 9:1 to the cation; weigh 1.9192g of a cross-linking agent methylenebisacrylamide with a mass ratio of 5:1 to acrylamide S...
Embodiment 3
[0038] A carbon quantum dot modified n-n type MFe 12 o 19 / CeO 2 The preparation method of magnetic separation photocatalyst comprises the following steps:
[0039] Step 1: Weigh 50g of glucose and dissolve it in 80mL of aqueous solution. After it is completely dissolved, transfer it to a reaction kettle lined with polytetrafluoroethylene, and place the reaction kettle in a drying oven at a constant temperature of 180°C for 5 hours , to obtain water-soluble carbon quantum dots.
[0040] Step 2: Press SrFe 12 o 19 The mol ratio of Sr and Fe in the middle is that the ratio of Sr:Fe=1:12 takes by weighing soluble 0.2442g strontium nitrate, soluble 5.5938g ferric nitrate, takes by weighing and cation molar ratio is the chelating agent citric acid 4.7282g of 1.5:1; Weigh 20g of gel-collapsing agent glucose; weigh 9.5958g of acrylamide with a molar ratio of 9:1 to the cation; weigh 1.9192g of a cross-linking agent methylenebisacrylamide with a mass ratio of 5:1 to acrylamide S...
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