Unlock instant, AI-driven research and patent intelligence for your innovation.

Technology for preparing carbon molecular sieve binder from PF waste resin

A binder preparation and waste resin technology, which is applied in the field of carbon molecular sieve binder preparation from PF waste resin, can solve the problems of resource waste and achieve the effects of avoiding waste, ensuring production quality and good coating effect

Pending Publication Date: 2020-05-29
爱克太尔新材料(南京)有限公司
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Aiming at the deficiencies of the prior art, the present invention provides a process for preparing carbon molecular sieve binders from waste PF resins, which has the advantages of recycling waste and improving the production quality of carbon molecular sieves, and solves the problem of thermosetting phenolic resin waste as a solid in the prior art. Hazardous wastes are processed, resulting in waste of resources

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] PF waste resin prepares carbon molecular sieve binder preparation process, comprises the raw material of following weight portion:

[0026] 20 parts of walnut shells, 30 parts of sodium bicarbonate powder, 25 parts of petroleum ether, 35 parts of fatty alcohol polyoxyethylene ether sodium sulfate, 15 parts of modified thermosetting phenolic resin and 30 parts of deionized water;

[0027] The modified thermosetting phenolic resin is prepared by the following method: add uncured phenolic resin waste into the stirring tank, then slowly add ethanol water with a volume fraction of 30% into the stirring tank, and stir during the addition process to adjust the phenolic resin The viscosity of the waste is in the range of 1800cps@25°C, and the modified thermosetting phenolic resin can be obtained.

[0028] PF waste resin prepares carbon molecular sieve binder preparation process, comprises the following steps:

[0029] S1: Add walnut shells into a ball mill and grind them evenl...

Embodiment 2

[0034] PF waste resin prepares carbon molecular sieve binder preparation process, comprises the raw material of following weight portion:

[0035] 25 parts of walnut shells, 35 parts of sodium bicarbonate powder, 28 parts of petroleum ether, 38 parts of fatty alcohol polyoxyethylene ether sodium sulfate, 20 parts of modified thermosetting phenolic resin and 35 parts of deionized water;

[0036] The modified thermosetting phenolic resin is prepared by the following method: add uncured phenolic resin waste into the stirring tank, then slowly add ethanol water with a volume fraction of 32% into the stirring tank, and stir during the addition process to adjust the phenolic resin The viscosity of the waste is in the range of 2000cps@25°C, and the modified thermosetting phenolic resin can be obtained.

[0037] PF waste resin prepares carbon molecular sieve binder preparation process, comprises the following steps:

[0038] S1: Add walnut shells into a ball mill and grind them evenl...

Embodiment 3

[0043] PF waste resin prepares carbon molecular sieve binder preparation process, comprises the raw material of following weight portion:

[0044] 30 parts of walnut shells, 40 parts of sodium bicarbonate powder, 30 parts of petroleum ether, 40 parts of fatty alcohol polyoxyethylene ether sodium sulfate, 25 parts of modified thermosetting phenolic resin and 40 parts of deionized water;

[0045] The modified thermosetting phenolic resin is prepared by the following method: add uncured phenolic resin waste into the stirring tank, then slowly add ethanol water with a volume fraction of 35% into the stirring tank, and stir during the addition process to adjust the phenolic resin The viscosity of the waste is in the range of 2500cps@25°C, and the modified thermosetting phenolic resin can be obtained.

[0046] PF waste resin prepares carbon molecular sieve binder preparation process, comprises the following steps:

[0047] S1: Add walnut shells into a ball mill and grind them evenl...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
Granularityaaaaaaaaaa
Granularityaaaaaaaaaa
Granularityaaaaaaaaaa
Login to View More

Abstract

The invention relates to the technical field of carbon molecular sieves, and discloses a technology for preparing a carbon molecular sieve binder from PF waste resin. The carbon molecular sieve binderis prepared from, by weight, 20 to 30 parts of walnut shells, 30 to 40 parts of an inorganic foaming material, 25 to 30 parts of a physical foaming material, 35 to 40 parts of a surfactant, 15 to 25parts of modified thermosetting phenolic resin and 30 to 40 parts of deionized water. The modified thermosetting phenolic resin is prepared by the following steps: adding uncured phenolic resin wasteinto a stirring tank, slowly adding ethanol water with the volume fraction of 30-35% into the stirring tank, stirring in the adding process, and adjusting the viscosity of the phenolic resin waste tobe 1500-2500 cps at 25 DEG C to obtain the modified thermosetting phenolic resin. The inorganic foaming material is sodium bicarbonate powder. The physical foaming material is petroleum ether. According to the technology for preparing the carbon molecular sieve binder from the PF waste resin, phenolic resin waste is effectively recycled, resource waste is avoided, and the production quality of thecarbon molecular sieve is guaranteed.

Description

technical field [0001] The invention relates to the technical field of carbon molecular sieves, in particular to a process for preparing carbon molecular sieve binders from waste PF resins. Background technique [0002] After a long period of storage, the thermosetting phenolic resin waste gradually increases in viscosity and water solubility gradually attenuates. At present, the main treatment method is to treat it as solid hazardous waste. On the one hand, this treatment method wastes resources. The manufacturer has brought economic losses. Considering the current production process of carbon molecular sieves in the market, thermosetting phenolic resin is used as the adhesive of the base material (foaming material) in the production process of carbon molecular sieves. Such adhesives are required to have A certain initial viscosity is used to carry out extrusion granulation, and the existing phenolic resin waste (uncured) is considered to reduce the viscosity of the phenoli...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C01B32/05C08L97/02C08L61/14C08J9/36C08J9/08C08J9/14C08G8/28
CPCC01B32/05C08J9/36C08J9/08C08J9/142C08L97/02C08G8/28C08J2203/02C08J2203/184C08J2397/02C08L61/14
Inventor 刘壮林张茜
Owner 爱克太尔新材料(南京)有限公司