Biochar-paraffin phase change heat storage material and preparation method thereof
A phase change heat storage material, biochar technology, applied in heat exchange materials, chemical instruments and methods, sustainable manufacturing/processing, etc. Surface activity and the effect of improving comprehensive mechanical properties
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Embodiment 1
[0022] In this example, the biochar-paraffin phase change heat storage material and its preparation method are as follows:
[0023] (1) Shred the recycled waste crop stalks to a particle size of 3mm.
[0024] (2) Heat the shredded straw to 800°C at a rate of 2°C / min in a tube furnace filled with nitrogen, and keep it warm for 2 hours to crack the straw into biochar materials, and then place the biochar materials at 500°C Surface oxidation treatment was carried out in a hot air atmosphere for 10 minutes.
[0025] (3) Put 85g of paraffin block with a melting point of 60°C into the cavity of the mold, weigh 15g of biochar and add it into the cavity, then heat the mold to 80°C and stir thoroughly to melt the paraffin block in the cavity It is evenly mixed with the biochar material, cooled and solidified naturally to obtain a phase change heat storage material.
[0026] The heat storage material has high phase change latent heat, good thermal conductivity, stable heat storage per...
Embodiment 2
[0028] In this example, the biochar-paraffin phase change heat storage material and its preparation method are as follows:
[0029] (1) Shred the recycled waste crop stalks to a particle size of 5 mm.
[0030] (2) Heat the shredded straw to 820°C at a rate of 3°C / min in a tube furnace filled with nitrogen, and keep it warm for 1 hour to crack the straw into biochar materials, and then place the biochar materials at 600°C Surface oxidation treatment was carried out for 8 minutes in a hot air atmosphere.
[0031] (3) Put 88g of paraffin block with a melting point of 60°C into the cavity of the mold, weigh 12g of biochar, then heat the mold to 85°C, and stir thoroughly to melt the paraffin block in the cavity and mix with the biochar. The carbon materials are evenly mixed, cooled and solidified naturally to obtain a phase change heat storage material.
[0032] The heat storage material has high phase change latent heat, good thermal conductivity, stable heat storage performance...
Embodiment 3
[0034] In this example, the biochar-paraffin phase change heat storage material and its preparation method are as follows:
[0035] (1) Shred the recycled waste crop stalks to a particle size of 1 mm.
[0036] (2) Heat the shredded straw to 780°C at a rate of 1°C / min in a tube furnace filled with nitrogen, and keep it warm for 3 hours to crack the straw into biochar materials, and then place the biochar materials at 400°C Surface oxidation treatment was carried out for 12 minutes in a hot air atmosphere.
[0037] (3) Put 82g of paraffin block with a melting point of 60°C into the cavity of the mold, weigh 18g of biochar, then heat the mold to 75°C and stir thoroughly to melt the paraffin block in the cavity and mix with the biochar. The carbon materials are evenly mixed, cooled and solidified naturally to obtain a phase change heat storage material.
[0038] The heat storage material has high phase change latent heat, good thermal conductivity, stable heat storage performanc...
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