Composite coating diaphragm with consistent pore diameter and preparation method thereof
A composite coating and coating technology, which is applied to electrical components, non-aqueous electrolyte batteries, circuits, etc., can solve the problems of reducing battery energy density, increasing diaphragm volume, quality, and battery electrical performance degradation, so as to reduce battery internal resistance , Improve cycle life, charge and discharge efficiency, and improve heat resistance
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[0022] Example 1
[0023] see figure 1 , This embodiment 1 provides a composite coating diaphragm, including: a base film 1 and a composite coating 2 coated on the surface of the base film; and the composite coating 2 contains polymer composite particles 3 and a ceramic composite Particles 4 to keep the pore size of the composite coating 2 consistent with the base film 1.
[0024] Optionally, the mass ratio of the polymer composite particles 3 to the ceramic composite particles 4 is 1:(0.5-20), and may be 1:5 or 1:10.
[0025] Optionally, the base film 1 includes a polypropylene film, a polyethylene film, or a multilayer composite film of both; and the base film contains micropores with a pore diameter of 0.01 μm to 0.8 μm.
[0026] Optionally, the polymer composite particles 3 include: polymer particles of at least two particle sizes, with particle sizes ranging from 0.1 μm to 4 μm and 4 to 8 μm, respectively; and the mass ratio of the two is 1: (0.1-10 ). The polymer composite par...
Example Embodiment
[0029] Example 2
[0030] Such as figure 2 As shown, on the basis of Example 1, this Example 2 also provides a method for preparing a composite coating diaphragm, including: preparing a composite coating slurry; coating the composite coating slurry on the surface of the base film; And drying to obtain a composite coated diaphragm.
[0031] Specifically, the composite coating slurry includes the following parts by mass of raw materials: deionized water: 50-95 parts; polymer composite particles: 1-40 parts; ceramic composite particles: 1-45 parts; binder: 1-20 parts; dispersant: 0.1-25 parts; wetting agent: 0.1-15 parts; stabilizer: 0.5-30 parts; and other additives: 0.1-10 parts.
[0032] Optionally, the composite coating slurry includes the following parts by mass of raw materials: deionized water: 80 parts; polymer composite particles: 20 parts; ceramic composite particles: 25 parts; binder: 15 parts; dispersant : 5 parts; wetting agent: 12 parts; stabilizer: 20 parts; and other...
Example Embodiment
[0036] Example 3
[0037] Mix 65 parts of deionized water, 0.91 parts of first polymer particles, 0.19 parts of second polymer particles, 3.64 parts of first ceramic particles, 0.36 parts of second ceramic particles, 4 parts of binder, 3 parts of dispersant, 2 parts of The wetting agent, 3 parts of stabilizer, and 3 parts of other additives are mixed uniformly to prepare a composite coating slurry.
[0038] The particle size of the first polymer particle is 0.1μm, the particle size of the second polymer particle is 4μm, the mass ratio of the two is 1:0.1, the initial particle size of the polymer is 0.1-0.5μm; the particle size of the first ceramic particle is 0.1μm, The particle size of the second ceramic particles is 0.6 μm, and the ratio is 1:0.1; wherein, the mass ratio of polymer particles to ceramic particles is 1:4.
[0039] Using polyethylene film as the substrate, the composite coating slurry was coated by a top coating process, where the top coating process was micro-gravur...
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