Preparation method of fluorinated carbon nitride with high fluorine content
A technology of reducing carbon nitride and fluorine content, which is applied in the field of preparation of fluorinated carbon nitrogen, can solve the problems of increased production costs and threats to the health of operators, and achieves the advantages of reduced production costs, mild fluorination, and safe operation Effect
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Embodiment 1
[0017] Embodiment 1: the structure of the support plate
[0018] The structure of the support plate is as figure 1 As shown, it includes three cylindrical support feet and a circular tray fixed on the three support feet, and both the support feet and the tray are made of quartz material.
Embodiment 2
[0019] Embodiment 2: Preparation of fluorine-doped graphite phase carbon nitride
[0020] Take 1g of xenon difluoride and place it on the bottom of the polytetrafluoroethylene inner cup, take 0.1g of graphite phase carbon nitride and place it on the support plate of the structure described in Example 1, then place it in the polytetrafluoroethylene inner cup, cover the inner Then put the polytetrafluoroethylene inner cup into the stainless steel outer tank of the high-pressure digestion tank, tighten the stainless steel cover, then place it in an oven, and react at a constant temperature of 200 ° C for 8 hours. After the reaction, naturally cool to room temperature to obtain fluorine Doped graphitic carbon nitride.
Embodiment 3
[0021] Embodiment 3: Preparation of fluorine-doped graphite phase carbon nitride
[0022] Repeat Example 2, the difference is that the amount of xenon difluoride is 2g.
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