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Softening agent with high stability, low color change and phenol yellowing resistance and preparation method thereof

A technology of anti-phenol yellowing agent and softener, which is applied in the field of high stability and low discoloration anti-phenol yellow softener and its preparation, can solve the problems of insufficient smoothness, poor alkali resistance, large storage phenol yellow, etc., and achieve hand feeling Soft and comfortable, excellent high temperature resistance, yellowing and fading effect

Pending Publication Date: 2020-08-18
GUANGDONG CHUANHUA FULIAN FINE CHEM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the amount of softener used in my country is large, and there are many varieties. It has gradually evolved from traditional fatty acid amide compounds to silicone polymers. However, in actual processing and use, a single variety is often difficult to meet customer needs.
Non-silicon softeners feel fluffy, cheap, but not smooth enough, high temperature resistance, and alkali resistance are relatively poor: Silicone softeners have excellent hand feel, but are prone to silicone oil spots, and with the increase of ammonia value and organic solvents Excessive use, usually the color of the cloth surface becomes larger, and the storage phenol yellow becomes larger during packaging and transportation. This phenomenon seriously plagues the printing and dyeing processing factories.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A preparation method of a softener with high stability and low discoloration and anti-phenol yellow, in parts by weight, comprising the following steps:

[0023] Add 10 parts of oleic acid and 5 parts of fatty alcohol polyoxyethylene ether O-25 to 40 parts of deionized water, raise the temperature to 70°C, heat and stir for 60 minutes to form a uniform emulsion, then cool down to 30°C, and add 10 parts of low yellowing Block silicone oil and 5 parts of sulfonate type anti-phenol yellowing agent were stirred evenly for 20 minutes to obtain the softener.

[0024] The softening agent prepared in this embodiment is resistant to high temperature, 5g / L soda ash and 10g / L sodium sulfate at room temperature, and does not float oil and does not stick to rollers.

Embodiment 2

[0026] A preparation method of a softener with high stability and low discoloration and anti-phenol yellow, in parts by mass, comprising the following steps:

[0027] Add 15 parts of alkali-resistant soft flakes and 8 parts of fatty alcohol and ethylene oxide condensate dispersant W into 54 parts of deionized water, raise the temperature to 75°C, heat and stir for 75 minutes to form a uniform emulsion, then cool down to 35°C, add 10 1 part of low-yellowing block silicone oil and 5 parts of sulfonate type anti-phenol yellowing agent, and stirred evenly for 20 minutes to obtain the softener.

[0028] The softening agent prepared in this embodiment is resistant to high temperature, 5g / L soda ash and 10g / L sodium sulfate at room temperature, and does not float oil and does not stick to rollers.

Embodiment 3

[0030] A preparation method of a softener with high stability and low discoloration and anti-phenol yellow, in parts by mass, comprising the following steps:

[0031] Add 20 parts of alkali-resistant soft flakes and 10 parts of fatty alcohol and ethylene oxide condensate dispersant IW into 70 parts of deionized water, raise the temperature to 80°C, heat and stir for 90 minutes to form a uniform emulsion, then cool down to 40°C, add 20 parts of low-yellowing block silicone oil and 10 parts of carboxylate type anti-phenol yellowing agent were stirred evenly for 30 minutes to obtain the softener.

[0032] The softening agent prepared in this embodiment is resistant to high temperature, 5g / L soda ash and 10g / L sodium sulfate at room temperature, and does not float oil and does not stick to rollers.

[0033] Taking the softening agent obtained in Example 2 as an example, it is applied to cotton knitted fabrics, brocade cotton fabrics, and polyester cotton fabrics respectively with ...

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PUM

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Abstract

The invention discloses a softening agent with high stability, low color change and phenol yellowing resistance and a preparation method thereof. The softening agent is prepared from the following components in parts by weight:10-20 parts of alkali-resistant soft sheets, 5-10 parts of a dispersion stabilizer, 10-20 parts of low yellowing block silicone oil, 5-10 parts of phenol yellowing resistance agent and 40-70 parts of deionized water. By optimizing reasonable raw materials, the softener overcomes the difficulty that a cationic softener and an anionic phenol yellowing resistance agent areprone to generating ionic reaction, has good stability, excellent high temperature resistance, shear resistance and soft and comfortable hand feeling, is smaller in color yellowing and is suitable forthe finishing of white or light-colored fabrics; and meanwhile, the softening agent can reach the fourth level in the storage and phenol yellowing resistance effects of cotton and blended fabrics ofthe cotton, and the export requirements are met.

Description

technical field [0001] The invention relates to a softener with high stability, low discoloration and anti-phenol yellow and a preparation method thereof, belonging to the field of textile finishing agents. Background technique [0002] Softener is a conventional auxiliary agent often used in the finishing process of the printing and dyeing industry. It is a textile chemical product that can give clothes and fabrics a smooth and soft feel. At present, the amount of softeners used in my country is large and there are many varieties. They have gradually evolved from traditional fatty acid amide compounds to silicone polymers. However, in actual processing and use, a single variety is often difficult to meet the needs of customers. Non-silicon softeners feel fluffy, cheap, but not smooth enough, high temperature resistance, and alkali resistance are relatively poor: Silicone softeners have excellent hand feel, but are prone to silicone oil spots, and with the increase of ammoni...

Claims

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Application Information

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IPC IPC(8): D06M15/647D06M13/203D06M15/53D06M13/256D06M13/17D06M13/184D06M101/06D06M101/32D06M101/34
CPCD06M15/647D06M13/203D06M15/53D06M13/256D06M13/17D06M13/184D06M2101/06D06M2101/32D06M2101/34D06M2200/50D06M2200/25
Inventor 黄武欢杨中新
Owner GUANGDONG CHUANHUA FULIAN FINE CHEM CO LTD
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