A method for preparing transparent conductive film from carboxyl functionalized graphene
A transparent conductive film, graphene technology, applied in the equipment, chemical instruments and methods for manufacturing conductive/semiconductive layers, conductive materials dispersed in non-conductive inorganic materials, etc., can solve the problem of low market share, technology Maturity and industrial production have not been completely opened up, etc., to achieve the effect of enhancing overall flexibility and electrical conductivity
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0026] (1) Measure 50 parts of graphene oxide slurry into the reaction kettle, stir and disperse with high-speed machinery for 5 minutes, then add 5 parts of a mixed solution of sulfuric acid and silver nitrate with a volume fraction ratio of 1:3, and continue stirring for 10 minutes until mixed Evenly, the reaction kettle was transferred to an ice-water bath environment, and the ultrasonic equipment with a power of 800W was used to assist the reaction for 3h. After the reaction, the solution was filtered with a Buchner funnel, and the filter cake was washed repeatedly with 5wt% dilute hydrochloric acid solution and deionized water for 3- Five times, the filter cake was dispersed into deionized water to prepare a carboxy-functionalized graphene dispersion with a concentration of 5 mg / mL.
[0027] (2) Adjust the optimum film-forming viscosity of the carboxyl-functionalized graphene dispersion to 8000mPa·s, adopt the scraping method to form the film, select the PET film substrate...
Embodiment 2
[0030] (1) The preparation method of the carboxyl-functionalized graphene dispersion is the same as in Example 1.
[0031] (2) Adjust the optimum film-forming viscosity of the carboxyl-functionalized graphene dispersion to 8000mPa·s, adopt the scraping method to form the film, select the PET film substrate with the release force of 15g / 25mm as the film-forming substrate, and adjust the size of the scraper accurately 0.20mm, after coating and forming a film, put it into an oven at 80°C for drying treatment to obtain a carboxyl-functionalized graphene film, and peel the film from the substrate by mechanical rolling.
[0032] (3) The preparation method of the graphene transparent conductive film is the same as that in Example 1.
Embodiment 3
[0034] (1) The preparation method of the carboxyl-functionalized graphene dispersion is the same as in Example 1.
[0035] (2) Adjust the optimum film-forming viscosity of the carboxyl-functionalized graphene dispersion to 8000mPa·s, adopt the scraping method to form the film, select the PET film substrate with the release force of 15g / 25mm as the film-forming substrate, and adjust the size of the scraper accurately 0.50mm, after coating and forming a film, put it into an oven at 80°C for drying treatment to obtain a carboxyl-functionalized graphene film, and peel the film from the substrate by mechanical rolling.
[0036] (3) The preparation method of the graphene transparent conductive film is the same as that in Example 1.
PUM
| Property | Measurement | Unit |
|---|---|---|
| thickness | aaaaa | aaaaa |
| viscosity | aaaaa | aaaaa |
| thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More