A kind of anti-fibrosis drug sustained-release coating and preparation method thereof
An anti-fibrosis and drug technology, applied in coatings, drug delivery, pharmaceutical formulations, etc., can solve the problems of complex preparation process and poor biocompatibility, and achieve simple preparation method, good biocompatibility, control Effect of early release rate
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Embodiment 1
[0033] 1. Add 0.5g of bovine serum albumin, 0.7g of tris(2-carboxyethyl)phosphine hydrochloride and 0.1g of hyaluronic acid into 100mL of deionized water, mix well, and adjust the pH to 4.5 with sodium hydroxide to obtain impregnation liquid; the concentration of bovine serum albumin in the soaking liquid is 5 mg / mL, the concentration of tris (2-carboxyethyl) phosphine hydrochloride is 7 mg / mL, and the concentration of hyaluronic acid is 1 mg / mL.
[0034] 2. Alternately clean the silicone catheter with ethanol and acetone, ultrasonically clean it with deionized water for 10 minutes, blow dry with nitrogen, and then spray and fix 10 mg / mL rapamycin ethanol solution on the surface of the silicone catheter to obtain rapamycin-coated The silicone catheter of the drug drug, wherein the spraying process parameters are: ultrasonic frequency is 120kHz, ultrasonic power is 2W, the flow rate of ultrasonic spraying solution is 1mL / min, the rotation speed of the driving equipment is 300r / m...
Embodiment 2
[0038]In step 1 of this example, add 1 g of bovine serum albumin, 0.7 g of tris(2-carboxyethyl)phosphine hydrochloride and 0.4 g of hyaluronic acid into 100 mL of deionized water, mix well, and adjust the pH with sodium hydroxide To 4.5, obtain the dipping solution; the concentration of bovine serum albumin in the dipping solution is 10mg / mL, the concentration of tris (2-carboxyethyl) phosphine hydrochloride is 7mg / mL, the concentration of hyaluronic acid is 4mg / mL mL. Other steps were the same as in Example 1, forming a sustained-release coating of rapamycin on the surface of the silicone catheter.
Embodiment 3
[0040] In step 1 of this example, add 0.5 g of bovine serum albumin, 0.7 g of tris(2-carboxyethyl)phosphine hydrochloride and 0.1 g of alginic acid into 100 mL of deionized water, mix well, and adjust the pH with sodium hydroxide To 4.5, obtain the soaking solution; the concentration of bovine serum albumin in the soaking solution is 5 mg / mL, the concentration of tris (2-carboxyethyl) phosphine hydrochloride is 7 mg / mL, and the concentration of alginic acid is 1 mg / mL . Other steps were the same as in Example 1, forming a sustained-release coating of rapamycin on the surface of the silicone catheter.
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