A Soil Leakage Monitoring Technology of Oil Storage Tank Using Magnetic Tracer
A tracer and oil storage tank technology, which is applied in the field of soil penetration detection of oil storage tanks, can solve the problem that oil leakage cannot be prevented, and oil storage tank leakage and small leakage cannot be detected timely and accurately. Oil storage tank leakage does not have real-time online monitoring and alarm functions, and achieves the effect of wide monitoring range, high positioning accuracy and high sensitivity
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Embodiment 1
[0061] A preparation method of a magnetic tracer, comprising:
[0062] Step 1, take FeC1 with a molar ratio of 2:1 3 ·6H 2 O and FeC1 2 ·4H 2 0, then add distilled water according to the material-to-liquid ratio of 1g:15mL, and stir the reaction for 30min at 70°C. After the reaction, add ammonia water according to the material-to-liquid ratio of 1g:3mL to make the magnetic Fe in the reaction system 3 O 4 Nanoparticles are precipitated and ready for use;
[0063] Step 2, magnetic Fe with a mass ratio of 1:18 3 O 4 Nanoparticles and glucose were added to deionized water, sonicated for 20 min, and reacted at 200 °C for 3 h. After natural cooling, the product was first washed with deionized water for 5 times, then washed with ethanol for 5 times, and vacuum-dried to obtain Fe. 3 O 4 @C microspheres;
[0064] Step 3, by 20wt% Fe 3 O 4 @C microspheres were dispersed in Augeo SL-191 solvent, followed by addition of glycidyl methacrylate, triethylamine and hydroquinone, n(F...
Embodiment 2
[0069] A preparation method of a magnetic tracer, comprising:
[0070] Step 1, take FeC1 with a molar ratio of 2:1 3 ·6H 2 O and FeC1 2 ·4H 2 0, then add distilled water according to the material-to-liquid ratio of 1g:12mL, and stir the reaction at 65°C for 45min. After the reaction, add ammonia water according to the material-to-liquid ratio of 1g:4mL to make the magnetic Fe in the reaction system 3 O 4 Nanoparticles are precipitated and ready for use;
[0071] Step 2, magnetic Fe with a mass ratio of 1:24 3 O 4Nanoparticles and glucose were added to deionized water, sonicated for 30 min, and reacted at 180 °C for 5 h. After natural cooling, the product was first washed with deionized water 3 times, then washed with ethanol 3 times, and dried in vacuum to obtain Fe 3 O 4 @C microspheres;
[0072] Step 3, by 15wt% Fe 3 O 4 @C microspheres were dispersed in Augeo SL-191 solvent, followed by addition of glycidyl methacrylate, triethylamine and hydroquinone, n(Fe 3 O ...
Embodiment 3
[0077] A preparation method of a magnetic tracer, comprising:
[0078] In step 2, magnetic Fe with a mass ratio of 1:24 was 3 O 4 Nanoparticles and glucose were added to deionized water, then gluconic acid with 0.6 wt % glucose was added, sonicated for 30 min, and reacted at 180 °C for 5 h. After natural cooling, the product was washed three times with deionized water, and then Washed with ethanol 3 times and dried under vacuum to obtain Fe 3 O 4 @C Microspheres; the rest are the same as in Example 2.
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