Preparation method of aerospace special high-performance composite material presoak
A technology for aerospace and composite materials, which is applied in the field of preparation of high-performance composite material pre-dipping solution for aerospace, can solve the problems of polluted processing environment, high price, and increased material processing cost.
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Embodiment 1
[0034] 1. Preparation of prepreg:
[0035] (1) Pretreatment of carbon fiber: Place the carbon fiber in an oven at 110°C for 12 hours, and then heat it at 400°C for 3 hours;
[0036] (2) Preparation of acrylamide-acrylate resin emulsion: Dissolve 180mmol of acrylamide and 60mmol of hydroxypropyl acrylate in water to obtain a monomer aqueous solution, heat to 70°C for 5h, and add ammonium persulfate aqueous solution (with ammonium persulfate By mass, 10 mmol), after the dripping is completed, the reaction is kept warm, and the reaction is completed to obtain an acrylamide-acrylate resin emulsion;
[0037] (3) Preparation of modified acrylamide-acrylic resin: Dissolve 10mmol of bromooxime ether in methanol to obtain the bromooxime ether solution, add the bromooxime ether solution to the acrylamide-acrylate resin emulsion prepared above, and heat React at 60°C for 5 hours, and add potassium carbonate aqueous solution (based on the mass of potassium carbonate, 10.5 mmol) dropwise. After ...
Embodiment 2
[0045] The only difference between Example 2 and Example 1 is that the immersion time during composite processing is modified to 15 minutes.
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