Composite conductive agent and preparation method thereof, and lithium ion battery
A technology of composite conductive agent and conductive agent, which is applied in the direction of battery electrodes, secondary batteries, circuits, etc., can solve the problems of carbon nanotube agglomerates being unable to disperse, low yield, and affecting the conductivity of carbon nanotubes, so as to improve electron transmission Efficiency, the effect of solving the difficulty of dispersion and reducing the probability of insufficient contact
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Embodiment 1
[0032] Step 1: Weigh 5g SWCNTs and 150g MWCNTs, add them to the reactor containing concentrated nitric acid solution, heat and stir at 50°C for 3h, cool, wash to pH ≈ 7, and dry to obtain acidified carbon nanotubes;
[0033] Step 2: The obtained acidified carbon nanotubes were ball milled with 1.2Kg SP for 24h, fully mixed, and then ultrasonically and stirred to disperse in 67.75Kg of Zn(NO) with a mass concentration of 0.5wt.%. 3 ) 2 In anhydrous methanol, use ammonia water to adjust PH ≈ 9, leave it to age for 12 hours, and obtain a mixed solution;
[0034] Step 3: Slowly add 800 g of 2-methylimidazole into the mixed solution in Step 2 under stirring condition, and stir for 6 hours to obtain a precipitate, which is centrifuged, washed, and dried at 80°C to obtain a solid powder;
[0035] Step 4: Place the solid powder obtained in Step 3 into pure N 2 Pyrolyze at 800°C for 2 hours in a gas environment, and the heating rate is 5°C / min to obtain a black powder, then pickle th...
Embodiment 2
[0040] Step 1: Weigh 5g of SWCNTs and 300g of MWCNTs, add them to a reactor containing concentrated nitric acid solution, heat and stir at 50°C for 3 hours, cool, wash to pH ≈ 7, and dry to obtain acidified carbon nanotubes;
[0041] Step 2: The obtained acidified carbon nanotubes were ball milled with 2.44Kg SP for 24h, fully mixed, and then ultrasonically and stirred to disperse in 122Kg of Zn(NO 3 ) 2 In anhydrous methanol, use ammonia water to adjust PH ≈ 9, leave it to age for 24 hours, and obtain a mixed solution;
[0042] Step 3: Slowly add 1.22Kg of 2-methylimidazole into the mixture in Step 2 under stirring condition, and stir for 6 hours to obtain a precipitate, which is centrifuged, washed, and dried at 80°C to obtain a solid powder;
[0043] Step 4: Place the solid powder obtained in Step 3 into pure N 2 Pyrolyze at 900°C for 1 hour in a gas environment with a heating rate of 5°C / min to obtain a black powder, then pickle the black powder in a dilute hydrochloric ...
Embodiment 3
[0048] Step 1: Weigh 5g of SWCNTs and 250g of MWCNTs, add them to a reactor containing concentrated nitric acid solution, heat and stir at 50°C for 3 hours, cool, wash to pH ≈ 7, and dry to obtain acidified carbon nanotubes;
[0049] Step 2: The obtained acidified carbon nanotubes were ball milled with 1.54Kg SP for 24h, fully mixed, and then ultrasonically and stirred to disperse in 67.75Kg of Zn(NO 3 ) 2 In anhydrous methanol, use ammonia water to adjust PH ≈ 9, leave it to age for 12 hours, and obtain a mixed solution;
[0050] Step 3: Slowly add 945g of 2-methylimidazole into the mixed solution of Step 2 under stirring condition, stir and react for 6h to obtain a precipitate, which is centrifuged, washed, and dried at 80°C to obtain a solid powder;
[0051] Step 4: Place the solid powder obtained in Step 3 into pure N 2 Pyrolyze at 600°C for 2 hours in a gas environment, and the heating rate is 5°C / min to obtain a black powder, then pickle the black powder in a dilute hy...
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