Application of methyl genipin in preparation of medicine for treating or preventing obesity and obesity metabolic syndromes
A technology for methyl genipin and metabolic syndrome, applied in metabolic diseases, drug combinations, pharmaceutical formulas, etc., can solve problems such as limiting therapeutic effects, and achieve the effects of enhancing therapeutic effects, reducing liver damage effects, and good therapeutic effects
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Embodiment 1
[0027] Embodiment 1: the preparation of genipin methyl
[0028] Take 100g of genipin, dissolve it in 300mL of methanol, quickly add 300mL of 2mol / L methanolic hydrochloric acid solution under stirring, continue to stir and react at room temperature for 10min, immediately pour it into water saturated with ethyl acetate, mix well, and use Ethyl acetate was extracted twice, the organic layers were combined, washed with water five times, and evaporated to dryness under reduced pressure. The residue was subjected to silica gel column chromatography and eluted with petroleum ether-ethyl acetate mixed solvent gradient to obtain genipin methyl.
Embodiment 2
[0029] Embodiment 2: Hepatotoxicity comparison between genipin and methylgenipin
[0030] 2.1 Materials
[0031] Genipin (Xi'an Lvzhiyin Biotechnology Co., Ltd.), and genipin methyl were prepared in Example 1.
[0032] 2.2 Administration and grouping
[0033] All medicines were made into 3 g / L gastric lavage solution with 0.5% carboxymethylcellulose sodium (CMC-Na) solution before use. DIO rats were randomly divided into 4 groups according to body weight; genipin group (n=10) by 20mg / kg / d ig; methylgenipin group (n=10) by 20mg / kg / d ig; blank group (n=10) and model group (n=10) ig equal amount of CMC-Na solution. Continuous administration for 4 weeks.
[0034] 2.3 Observation indicators
[0035] 2.3.1 Abnormal symptoms
[0036] The daily performance of experimental animals in each group was observed and recorded from time to time every day. Observe whether the animals have abnormal performance and symptoms before and after treatment.
[0037] 2.3.2 Body weight and Lee's...
Embodiment 3
[0063] Example 3: Pharmacodynamic study of genipin methyl, orlistat and their combination
[0064] 3.1 Materials
[0065] Orlistat Capsules (Chongqing Huasen Pharmaceutical Co., Ltd.), and genipin methyl are made by Example 1.
[0066] 3.2 Grouping and administration
[0067] Methylgenipin group (n=10) by 20mg / kg / d ig; orlistat group (n=10) by 20mg / kg / dig; orlistat+methylgenipin group: Listat: methyl genipin mass ratio (abbreviated as O: A) = 5:1, 2:1, 1:1, 1:2, 1:5, the total dosage remains orlistat + methyl Genipin=20mg / kg / d, ig, a total of 5 groups, each group n=10; model group (n=10) and blank group (n=10) ig equal amount of CMC-Na solution. Continuous administration for 4 weeks.
[0068] 3.3 Observation indicators
[0069] 3.3.1 Body weight and Lee's index
[0070] The animals were weighed once before and after treatment, and the body length (length from nose to anus) and abdominal circumference were accurately measured under anesthesia before sacrifice, according t...
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