Halogen-free flame-retardant modified hydrocarbon resin and preparation method thereof
A hydrocarbon resin and modification technology, applied in the field of halogen-free flame retardant modification and its preparation, can solve the harm caused to human health and ecological environment, and affect the electrical and mechanical properties of the sheet, as well as high dielectric constant and dielectric loss. problem, to achieve the effect of narrow reaction residence time, simple process and good flame retardant effect
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Embodiment 2
[0055] A halogen-free flame-retardant modified hydrocarbon resin, the halogen-free flame-retardant modified hydrocarbon resin is a mixture of hydrocarbon resin, a double bond-containing phosphate flame retardant, an initiator and a solvent through a microchannel reactor to mix and react and remove Part of the solvent is obtained;
[0056] Described hydrocarbon resin is styrene-butadiene resin, polybutadiene resin, polyisobutadiene resin, polypentadiene resin, styrene-butadiene copolymer, styrene-isobutadiene copolymer, styrene - Divinylbenzene copolymer, polystyrene, 2-methyl polystyrene, 3-methyl polystyrene, 4-methyl polystyrene, 2,4-diisopropyl polystyrene, 2, One or more mixtures of 4-dimethyl polystyrene, ethylene propylene copolymer and cycloolefin copolymer;
[0057] The double bond-containing phosphate flame retardant is one or a mixture of two or more of the following formulas (1) and (2):
[0058]
[0059] In formula (1): R 1 for -ch 2 -, -C 3 H 6 -, -C 2 H...
Embodiment 3
[0065] A halogen-free flame retardant modified hydrocarbon resin, the initiator is dicumyl peroxide, di-tert-butyl peroxide, tert-butyl peroxybenzoate, dicyclohexyl peroxydicarbonate, isopropyl One or more mixtures of benzene hydroperoxide and azobisisobutyronitrile.
Embodiment 4
[0067] A halogen-free flame retardant modified hydrocarbon resin, the microchannel reactors are Corning microchannel reactors, Shandong Haomai microchannel reactors, Suzhou Wenhao microreactors, Shanghai Sanwei microchannel reactors, and Mijing microchannel reactors. Any one of the technology microchannel reactor, Gongyi Yuhua microchannel reactor, and Fluke microchannel reactor, the others are the same as in Example 2, and are omitted.
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