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Growth method of silicon carbide crystal grown by pvt method

A growth method, a technology of silicon carbide, applied in chemical instruments and methods, single crystal growth, single crystal growth, etc., can solve the problems of crystal defects and low quality of silicon carbide crystal growth, so as to improve quality and reduce carbon inclusion defects , the effect of avoiding crystal defects

Active Publication Date: 2021-07-23
CEC COMPOUND SEMICON CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0014] In view of the above-mentioned shortcomings of the prior art, the object of the present invention is to provide a growth method for growing silicon carbide crystals by PVT method, which is used to solve the problem of silicon-rich vapor deposition on the crystal when the PVT method is used to form silicon carbide crystals in the prior art. The surface condenses into silicon droplets to form crystallization defects, resulting in problems such as lower quality of silicon carbide crystal growth

Method used

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  • Growth method of silicon carbide crystal grown by pvt method
  • Growth method of silicon carbide crystal grown by pvt method
  • Growth method of silicon carbide crystal grown by pvt method

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Experimental program
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Embodiment 1

[0056] As mentioned in the background technology, in the initial stage of silicon carbide crystal growth, the growth atmosphere is rich in gaseous silicon, and under the action of axial temperature gradient, the steam is transported to the low-temperature silicon carbide seed crystal region, and the saturated vapor pressure of the silicon-rich gas phase decreases, condensing into Liquid-phase silicon causes crystallization defects. In order to overcome this defect, gas that can react with silicon vapor at high temperature is usually introduced into the silicon carbide raw material to form silicide, thereby removing gas-phase silicon in the growth atmosphere. However, silicon carbide crystals produced by this method still have crystal defects.

[0057] Based on the above-mentioned problems and detailed analysis of various factors, the inventor determined that the main reason for the crystallization defects in silicon carbide crystals is that the uniformity of chlorine-containing...

Embodiment 2

[0071] This embodiment provides a method for growing silicon carbide crystals, which is realized based on the crucible for growing silicon carbide crystals by the PVT method described in Embodiment 1. For the beneficial effects that the crucible can achieve, please refer to Embodiment 1, as follows No longer.

[0072] Such as Figure 2 to Figure 4 As shown, the growth method comprises the steps of:

[0073] 1) Provide a crucible for growing silicon carbide crystals by PVT method as described in Embodiment 1, and place a silicon carbide raw material 7 on a porous graphite plate 3 in the crucible and place a silicon carbide seed above the accommodating chamber 12 of the crucible Crystal 6;

[0074] 2) Put the crucible into the silicon carbide single crystal growth chamber. The silicon carbide single crystal growth chamber is mainly used for heating. Generally, the silicon carbide single crystal growth temperature is above 2000°C, and eddy current heating is adopted, that is, ...

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Abstract

The invention provides a method for growing silicon carbide crystals by a PVT method, the method comprising: providing a crucible; placing a silicon carbide raw material and a seed crystal in the crucible; putting the crucible into a growth chamber and vacuuming it, and then introducing a protective gas , set the temperature of the chamber; when the temperature rises to the first preset temperature, the chlorine-containing gas is introduced through the degassing device in the crucible, the temperature rises to the second preset temperature, and the feeding is stopped or continued for the first preset time Chlorine-containing gas; the temperature rises to a third preset temperature, and after the silicon carbide crystals start to grow for a second preset time, silicon carbide crystals are obtained by annealing. This growth method can effectively control the release rate and uniformity of chlorine-containing gas, and avoid crystallization defects caused by the condensation of gas-phase silicon on the crystal surface; by controlling the time and flow rate of chlorine-containing gas, crystallization defects can be further avoided; the placement of porous graphite blocks It can make the excess chlorine-containing gas introduced and the carbon particles suspended in the growth atmosphere escape, and reduce the carbon inclusion defects in the crystal.

Description

technical field [0001] The invention relates to the technical field of silicon carbide crystal preparation, in particular to a method for growing silicon carbide crystals by a PVT method. Background technique [0002] Compared with silicon-based semiconductors, the third-generation semiconductors represented by silicon carbide have the characteristics of forbidden bandwidth, high saturated electron mobility, high breakdown electric field strength, and high thermal conductivity. They have high frequency, high temperature resistance, chemical corrosion resistance, High efficiency, strong radiation resistance, high pressure resistance and other superior performance, with the increasingly mature silicon carbide semiconductor preparation technology, will increasingly become an Supporting materials for core electronic devices in fields such as petroleum exploration and production. [0003] Silicon carbide crystal preparation methods include high temperature chemical vapor deposit...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C30B23/00C30B29/36
CPCC30B23/002C30B29/36
Inventor 陈豆薛卫明马远
Owner CEC COMPOUND SEMICON CO LTD
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