Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Efficient boiling heat transfer copper material and preparation method thereof

A boiling heat transfer and copper technology, applied in nanotechnology and other directions, can solve the problems of uncontrollable processing quality of nanowires, uncontrollable formation process, sharp increase in processing cost, etc., and achieve excellent boiling heat transfer performance and high critical heat flux density. , the effect of low superheat

Inactive Publication Date: 2021-01-05
SUZHOU INST OF NANO TECH & NANO BIONICS CHINESE ACEDEMY OF SCI
View PDF6 Cites 2 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although this improved processing technology can achieve in-situ growth of copper wires and has excellent boiling heat transfer performance, there are inevitable problems in this processing method: large-area processing cannot be realized due to the limitation of the template, and the processing cost increases with the template area. increase sharply; mechanical tight fit can easily lead to template fragmentation, resulting in uncontrollable processing quality of nanowires; the formed nanowires will randomly form clusters under capillary action, although the microcavities formed by such clusters are beneficial nucleation, but its formation process is uncontrollable
Therefore, how to develop highly efficient boiling heat transfer micro-nano copper materials with real commercial value and its processing technology still face great challenges.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Efficient boiling heat transfer copper material and preparation method thereof
  • Efficient boiling heat transfer copper material and preparation method thereof
  • Efficient boiling heat transfer copper material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0027] Another aspect of the embodiments of the present invention provides a method for preparing a high-efficiency boiling heat transfer copper material, which includes: combining a substrate as a working electrode with a counter electrode and a weakly alkaline copper salt electrolyte to form an electrochemical working system , and apply a reduction current between the working electrode and the counter electrode, and form a porous copper film on the surface of the substrate through an electrodeposition reaction. The porous copper film includes several copper nano cones, and the copper nano cones distributed between the plurality of copper nano cones Irregular open microcavities are interconnected to form a porous microcavity structure;

[0028] In addition, the copper nanocone is in the shape of a needle cone, with an average height of 3-8 μm, a bottom diameter of 500-2200 nm, and a tip diameter of 0-50 nm.

[0029] Further, the distribution density of the copper nano cones i...

Embodiment 1

[0047] This embodiment relates to a nano-cone structure high-efficiency boiling heat transfer copper material prepared by electrochemical deposition, which is used to enhance boiling heat transfer. Specific steps are as follows:

[0048] (1) Polish the surface of the copper test piece, rinse it with ultrapure water, and dry it with high-purity nitrogen. This step is to remove the surface oxide layer.

[0049] (2) The copper test piece processed in step (1) is used as the working electrode, placed in the weakly alkaline copper salt electrolyte solution, the platinum electrode is used as the counter electrode, and the silver / silver chloride is used as the reference electrode. The working electrodes are connected by wires, and a loop is formed between the counter electrode and the reference electrode. The distance between the counter electrode and the working electrode was controlled to be 60mm, and the constant voltage electrodeposition reaction was carried out in a constant t...

Embodiment 2

[0053] This embodiment relates to a nano-cone structure high-efficiency boiling heat transfer copper material prepared by electrochemical deposition, which is used to enhance boiling heat transfer. Specific steps are as follows:

[0054] (1) Polish the surface of the copper test piece, rinse it with ultrapure water, and dry it with high-purity nitrogen. This step is to remove the surface oxide layer.

[0055] (2) The copper test piece processed in step (1) is used as the working electrode, placed in the weakly alkaline copper salt electrolyte solution, the platinum electrode is used as the counter electrode, and the silver / silver chloride is used as the reference electrode. The working electrodes are connected by wires, and a loop is formed between the counter electrode and the reference electrode. The distance between the counter electrode and the working electrode was controlled to be 40mm, and the constant voltage electrodeposition reaction was carried out in a constant t...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
diameteraaaaaaaaaa
diameteraaaaaaaaaa
sizeaaaaaaaaaa
Login to View More

Abstract

The invention discloses an efficient boiling heat transfer copper material and a preparation method thereof. The surface of the efficient boiling heat transfer copper material is coated with a porouscopper film; the porous copper film comprises a plurality of copper nanocones; and irregular open micro-cavities distributed among the plurality of copper nanocones communicate with one another to form a porous micro-cavity structure. The preparation method comprises the following steps of: assembling a base material serving as a working electrode, a counter electrode and a weakly alkaline coppersalt electrolyte to form an electrochemical working system, applying a reduction current between the working electrode and the counter electrode, and forming a porous copper film on the surface of thebase material through an electrodeposition reaction. The efficient boiling heat transfer copper material disclosed by the invention has the advantages of higher heat exchange area, far more nucleation sites, more excellent boiling heat transfer performance, a higher boiling heat transfer coefficient, higher critical heat flux density, lower superheat degree of nucleate boiling onset, a simple andconvenient preparation process, easiness in reaction regulation and control and low cost; and the efficient boiling heat transfer copper material is suitable for industrial scale application.

Description

technical field [0001] The invention relates to a structure and a method for enhancing surface heat transfer, in particular to a high-efficiency boiling heat transfer micro-nano porous copper material and a preparation method thereof. Background technique [0002] With the development of miniaturization, integration, and high power of electronic devices, a severe test is put forward for high heat flow heat dissipation. Using existing or developing new micro-nano processing technology to develop micro-nano copper materials with better boiling heat transfer performance has become the focus of current research. In 2008, the team of Professor Peterson of the University of Colorado in the United States used the grazing angle deposition technology to in-situ grow copper nanorod arrays on the surface of copper and confirmed that it has efficient boiling heat transfer performance (Small, 2008, 4, 1084-1088). The surface of copper nanorods prepared by this method has countless micro...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C25D3/38B82Y40/00
CPCB82Y40/00C25D3/38
Inventor 高雪峰吴菲菲泽花姐
Owner SUZHOU INST OF NANO TECH & NANO BIONICS CHINESE ACEDEMY OF SCI
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products