Polyurethane material and preparation method thereof
A technology of polyurethane material and polyether, which is applied in the field of polyurethane material and its preparation, can solve problems such as heat preservation, flame retardancy, and lack of mechanical properties, and achieve the effects of excellent chemical properties, improved compressive strength, and low moisture permeability coefficient
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Embodiment 1
[0024] Raw materials for polyurethane preparation are proportioned in parts by mass:
[0025] serial number name number of copies 1 Poly(1,4-cyclohexanedimethanol adipate) 32 2 polycarbonate diol 43 3 1,4-Butanediol 4 4 Dibutyltin dilaurate 0.06 5 Low viscosity dimethyl silicone oil, methyl phenyl silicone oil 3 6 Silica powder 2.5
[0026] The preparation method is as follows:
[0027] S1. Add polycarbonate diol into the reaction kettle, stir, and heat at 100°C;
[0028] S2. The polycarbonate diol is vacuumized and dehydrated, and the moisture in the raw material and the system is measured by the Karl Fischer method until the moisture content is lower than 1%,;
[0029] S3. Put poly(1,4-cyclohexanedimethanol adipate), heat to 75°C, add dibutyltin dilaurate, low-viscosity dimethyl silicone oil, methylphenyl silicone oil, and react for 3 hours above, and carry out vacuum degassing;
[0030] S4. Add 1,4-butanediol an...
Embodiment 2
[0034] The preparation method is the same as in Example 1, and the raw materials for polyurethane preparation are proportioned in parts by mass:
[0035] serial number name number of copies 1 Poly(1,4-cyclohexanedimethanol adipate) 37 2 polycarbonate diol 46 3 1,4-Butanediol 5 4 Dibutyltin dilaurate 0.06 5 Low viscosity dimethyl silicone oil, methyl phenyl silicone oil 5 6 Silica powder 4
Embodiment 3
[0037] The preparation method is the same as in Example 1, and the raw materials for polyurethane preparation are proportioned in parts by mass:
[0038] serial number name number of copies 1 Poly(1,4-cyclohexanedimethanol adipate) 40 2 polycarbonate diol 20 3 1,4-Butanediol 3 4 Dibutyltin dilaurate 0.06 5 Low viscosity dimethyl silicone oil, methyl phenyl silicone oil 7 6 Silica powder 5
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