High-performance PVC plastic pipe and preparation method thereof
A plastic pipe, high-performance technology, applied in the field of high-performance PVC plastic pipe and its preparation, can solve the problems of unsatisfactory modification effect, product performance decline, lack of pertinence, etc., to improve physical and mechanical properties, improve processing plastic Enhanced performance and improved stability
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Embodiment 1
[0039] Preparation of MMA / S-nanomontmorillonite composites:
[0040] (1) Dissolve 100g of sodium montmorillonite in water, prepare a suspension with a mass fraction of 4%, raise the temperature to 75°C, add 25g of cetyltrimethylammonium bromide under stirring, and stir for 2 hours , standing for stratification, filtering, taking the precipitate, washing the precipitate with water, drying it in vacuum to constant weight, grinding and sieving to obtain organic nano-montmorillonite;
[0041] (2) Mix 25g of organic nano-montmorillonite with water and place it in a reactor. The amount of water used is 6 times the total volume of methyl methacrylate and styrene. Under nitrogen protection, heat and stir in a water bath at 80°C for 1h. , lower the temperature to 70°C, add 300g methyl methacrylate, 100g styrene and 12g dibenzoyl peroxide, continue the reaction for 6h, then raise the temperature to 85°C, and react for 2h. Precipitate, wash the precipitate with water and vacuum dry to c...
Embodiment 2
[0043] Preparation of MMA / S-nanomontmorillonite composites:
[0044] (1) Dissolve 200g of sodium montmorillonite in water, prepare a suspension with a mass fraction of 7%, raise the temperature to 85°C, add 70g of cetyltrimethylammonium bromide under stirring, and stir for 1h , standing for stratification, filtering, taking the precipitate, washing the precipitate with water, drying it in vacuum to constant weight, grinding and sieving to obtain organic nano-montmorillonite;
[0045] (2) 135g of organic nano-montmorillonite is mixed with water, placed in a reactor, the amount of water is 7 times the total volume of methyl methacrylate and styrene, under nitrogen protection, 85 ℃ water bath heating and stirring reaction 0.5 h, lower the temperature to 75°C, add 400g of methyl methacrylate, 100g of styrene and 20g of dibenzoyl peroxide, continue the reaction for 4h, then raise the temperature to 90°C, and react for 1h. The precipitate was taken, washed with water, and then vacu...
Embodiment 3
[0047] Preparation of MMA / S-nanomontmorillonite composites:
[0048] (1) Dissolve 100g of sodium montmorillonite in water, prepare a suspension with a mass fraction of 5%, heat up to 80°C, add 30g of cetyltrimethylammonium bromide under stirring, and stir for 1.5 h, standing for stratification, filtering, taking the precipitate, washing the precipitate with water, drying in vacuum to constant weight, grinding and sieving to obtain organic nano-montmorillonite;
[0049] (2) Mix 75g of organic nano-montmorillonite with water, place in a reactor, the amount of water is 7 times the total volume of methyl methacrylate and styrene, under nitrogen protection, heat and stir in a water bath at 80°C for 1h , lower the temperature to 70°C, add 350g methyl methacrylate, 100g styrene and 18g dibenzoyl peroxide, continue the reaction for 6h, then raise the temperature to 90°C, and react for 1h. Precipitate, wash the precipitate with water and vacuum dry to constant weight to obtain the MMA...
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