Binder solution for lithium ion battery electrode, slurry for lithium ion battery electrode, lithium ion battery electrode, and lithium ion battery
A lithium-ion battery and adhesive technology, which is applied to battery electrodes, non-aqueous electrolyte battery electrodes, lithium batteries, etc. Good elasticity, good capacity retention, and high adhesion
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[0218] Hereinafter, the present invention will be specifically described by way of examples and comparative examples. However, the description of the above-mentioned preferred embodiments and the following examples are provided for the purpose of illustration only, and are not provided for the purpose of limiting the present invention. Therefore, the scope of the present invention is not limited to the embodiments or examples specifically described in this specification, but is limited only by the scope of the claims. In addition, in each Example and a comparative example, unless otherwise indicated, numerical values, such as a part and %, are based on mass.
[0219] 1. Manufacture of (A) component
manufacture example 1
[0221] Add 1450g ion-exchanged water, 137.3g (1.5580mol) hydroxyethyl vinyl ether, 188.6g (1.3266mol) 50% acrylamide aqueous solution, 0.09g (0.0006 mol) sodium methallyl sulfonate (Metalyl sulfonate Natrium), after removing oxygen in the reaction system with nitrogen gas, the temperature was raised to 50°C. 2.3 g of 2,2'-azobis-2-amidinopropane dihydrochloride (2,2'-Azobis-2-Amijinopropane dihydrochloride) (manufactured by Nippon Chemical Co., Ltd., product name "NC-32"), 50 g of ion-exchanged water, heated up to 80° C. for 3 hours of reaction to obtain an aqueous solution containing a water-soluble polymer.
manufacture example 2
[0223] 550 g of ion-exchanged water was added to a reaction device equipped with a stirrer, a thermometer, a reflux condenser, and a nitrogen introduction pipe, and after removing oxygen in the reaction system with nitrogen, the temperature was raised to 80°C. 99.0g (1.1236mol) hydroxyethyl vinyl ether, 870.8g (6.1241mol) 50% acrylamide aqueous solution, 0.2g (0.0014mol) sodium methallyl sulfonate, 100g ion-exchanged water were added dropwise thereto simultaneously A mixed solution of 5.3 g of 2,2'-azobis-2-amidinopropane dihydrochloride (manufactured by Nippon Chemical Co., Ltd., product name "NC-32"), and 170 g of ion-exchanged water. It added dropwise over 3 hours while keeping the temperature at 80° C. to obtain an aqueous solution containing a water-soluble polymer.
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