Inter-layer bonding sheet for multi-layer board and preparation method and application of inter-layer bonding sheet
A technology of multi-layer boards and adhesive sheets, which is applied in the fields of application, chemical instruments and methods, coatings, etc., can solve the problem of difficulty in meeting the process requirements and use requirements of printed circuit boards, and the poor reliability of heat resistance of PTFE multi-layer board bonding , poor bonding performance between fluororesin and film materials, etc., to meet the needs of high-frequency signals, stability, fluidity and bonding performance, and strong interlayer bonding
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Embodiment 1
[0071] This embodiment provides an interlayer bonding sheet for a multilayer board, the preparation method of which is as follows:
[0072] (1) the PTFE substrate with a thickness of 0.5mm is cleaned with acetone, degreased, and dried; then it is placed in a low-temperature plasma generator, and the setting voltage is 3000V, the system vacuum is 155Pa, and the radio frequency power is 1kW. in N 2 、H 2 In the mixed atmosphere (N 2 、H 2 The volume ratio is 8:2) take out after processing 600s, obtain the PTFE substrate after surface plasma treatment;
[0073] (2) The upper and lower surfaces of the PTFE substrate after the surface plasma treatment obtained in step (1) are roll-coated with dielectric resin treatment solution I respectively to obtain a dielectric resin layer with a thickness of 25 μm on the upper and lower surfaces, and solidify at 180° C. for 2.5 h , to obtain the interlayer adhesive sheet for the multilayer board.
Embodiment 2
[0075] This embodiment provides an interlayer bonding sheet for a multilayer board, the preparation method of which is as follows:
[0076] (1) the PTFE substrate with a thickness of 0.9mm is cleaned with ethanol, degreased, and dried; then it is placed in a low-temperature plasma generator, and the setting voltage is 3000V, the system vacuum is 560Pa, and the radio frequency power is 3kW, In Ar, H 2 In a mixed atmosphere (Ar, H 2 The volume ratio is 9:1) and taken out after 240s treatment to obtain the PTFE substrate after surface plasma treatment;
[0077] (2) The upper and lower surfaces of the PTFE substrate after the surface plasma treatment obtained in step (1) are respectively roll-coated with dielectric resin treatment liquid I to obtain a dielectric resin layer with a thickness of 40 μm on the upper and lower surfaces, and solidify at 210°C for 2h. The interlayer adhesive sheet for the multilayer board was obtained.
Embodiment 3
[0079] This embodiment provides an interlayer bonding sheet for a multilayer board, the preparation method of which is as follows:
[0080] (1) the PTFE substrate with a thickness of 1.3mm is cleaned with ethanol, degreased, and dried; then it is placed in a low-temperature plasma generator, and the setting voltage is 6000V, the system vacuum is 1224Pa, and the radio frequency power is 5kW, Take it out after being treated in an Ar atmosphere for 60s to obtain a PTFE substrate after surface plasma treatment;
[0081] (2) the upper and lower surfaces of the PTFE substrate after the surface plasma treatment obtained in step (1) are roll-coated with dielectric resin treatment solution I respectively to obtain a dielectric resin layer with a thickness of 50 μm on the upper and lower surfaces, and solidify at 200° C. for 3 h, The interlayer adhesive sheet for the multilayer board was obtained.
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