A method to reduce the production cost of multi-arc chromium target

A production cost, chromium target technology, applied in vacuum evaporation plating, coating, sputtering plating and other directions, can solve the problems of high subsequent wire cutting costs, falling off, complicated procedures, etc., to save raw material input costs and bonding strength. High, easy-to-recover effect

Active Publication Date: 2021-08-06
江苏应用元素科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0013] Therefore, in view of the current process and industry's demand for continuous reduction in the cost of multi-arc chromium targets, it is mainly aimed at the high cost of the material at the connecting thread and there is no need to use chromium as the base material, the subsequent wire cutting costs are high, and the two processes of inlaying and brazing copper blocks Complicated and there are practical problems such as the risk of falling off caused by thermal expansion and contraction during the coating process. This invention provides a complete set of solutions to optimize the material utilization rate and processing method to the optimum level, which not only reduces the cost but also improves the reliability of product use. sex

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0035] First, according to the preparation process of the conventional circular chromium target, prepare a 20# steel ladle with an inner diameter of Φ123mm and a length of L;

[0036] Prepare 304 stainless steel chip briquettes with a density 10% higher than the tap density of chromium powder. Because the tap density of metal chromium powder with conventional particle size is 4.2g / cm 3 , so the pure and dry 304 stainless steel shavings are pressed into a density of 4.2*1.1=4.62g / cm by a hydraulic press 3 The briquette, the diameter of the briquette is Φ123-0.1mm, and the thickness is 17mm.

[0037] Packing sleeve: put 304 stainless steel briquettes in the bottom layer, then put the calculated weight of chromium powder and 304 stainless steel briquettes alternately, and put 304 stainless steel briquettes in the top layer. Put it on the vibrating table during the briquetting process, turn on the vibrating table, the amplitude is 3.5mm, the vibration frequency is 100-350 times / ...

Embodiment 1

[0043] A method for making a 2N5 pure multi-arc target with a diameter of Φ100*40mm;

[0044] Step 1. First, prepare the circular sheath, select 20# seamless steel pipe with a wall thickness of 2mm, its inner diameter is Φ123mm, and the length is 930mm; the cover is made of 2.5mm thick 304 cold-rolled stainless steel plate by spinning. The size of the steel pipe used for the sheathed exhaust pipe is Φ16mm in outer diameter and 2.5~3mm in wall thickness.

[0045] Step 2, preparing a 304 stainless steel chip briquette with a density 10% higher than the tap density of the chromium powder. The selected 304 stainless steel shavings must be pure and dry, without any pure iron and other impurities, to ensure that the compact is non-magnetic. Because the tap density of metal chromium powder with conventional particle size is 4.2g / cm 3 , so the pure and dry 304 stainless steel shavings are pressed into a density of 4.2*1.1=4.62g / cm by a hydraulic press 3 The briquette, the diameter ...

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Abstract

The invention provides a method for reducing the production cost of a multi-arc chromium target, comprising the following steps: step 1, preparing a No. 20 steel ladle; step 2, preparing a 304 stainless steel chip briquette with a density 10% higher than the tap density of chromium powder, Press the pure and dry 304 stainless steel shavings into a density of 4.62g / cm through a hydraulic press 3 Step 3, put the bottom layer of the ladle cover in step 1 into the 304 stainless steel chip briquette made in step 2; step 4, vacuum degassing; step 5, hot isostatic pressing: seal the step 4 The welded ladle cover is sent to the hot isostatic pressing machine for hot isostatic pressing; step six, machining the finished product. Using cheap and easy-to-obtain 304 stainless steel chips to replace expensive high-purity metal chromium can save about 25% of raw material input costs.

Description

technical field [0001] The invention belongs to the field of powder metallurgy, and in particular relates to a method capable of significantly reducing the processing cost of a multi-arc chromium target. Background technique [0002] Multi-arc ion plating technology is a kind of ion plating technology using cathodic arc evaporation source. In the 19th century, the American inventor Thomas Edison proposed the idea of ​​using vacuum arc for coating and applied for a US patent. After the 1980s, my country introduced a large number of equipment and technologies, and multi-arc ion plating has achieved rapid development. [0003] The basic components of multi-arc ion plating include vacuum coating chamber, cathode arc source, substrate, negative bias power supply, and vacuum system. Among them, the cathode arc source is the core of multi-arc ion plating, and the metal plasma generated by it automatically maintains the arc discharge between the cathode and the coating chamber. Th...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B22F3/15B22F3/24B22F5/10C23C14/32
CPCB22F3/15B22F3/24B22F5/10B22F2003/247C23C14/325
Inventor 彭凌剑彭方平彭夏元
Owner 江苏应用元素科技有限公司
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