Efficient heat conduction gasket and preparation method thereof
A thermally conductive gasket and high-efficiency technology, applied in the field of high-efficiency thermally conductive gaskets and their preparation, can solve the problems of insufficient flexibility and adhesion, poor thermal conductivity, etc., and achieve the advantages of improving thermal conductivity, reducing absorption, and reducing contact thermal resistance. Effect
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[0031] The embodiment of the present invention also provides a method for preparing the above-mentioned high-efficiency heat-conducting gasket, the method comprising the following steps:
[0032] Step 1, add the micron-scale carrier to the nano-scale thermally conductive filler with high thermal conductivity in a weight ratio of 95:5 to 85:15 into the high-speed mixer, and mix and disperse under the condition of a line speed of 40 to 70m / s 5 to 30 minutes to obtain a thermally conductive filler with a composite structure after high-speed dispersion;
[0033] Step 2, placing the high-speed dispersed composite structure heat-conducting filler and the one-dimensional structure-oriented heat-conducting material obtained in step 1 in a vacuum mixer, and vacuuming at 10-50°C for 10-30 minutes , after the air in the system is removed, stop the vacuum treatment;
[0034] Step 3: Mix vinyl polyorganosiloxane, silane coupling agent, terminal hydrogen-containing silicone oil, and cataly...
Embodiment 1
[0038] Step 1, 80 parts of modified spherical alumina (average particle size is 20 μm), 15 parts of modified spherical alumina (average particle size is 5 μm) and 5 parts of modified nano-graphene (average particle size is 200nm) are added respectively into a high-speed mixer (FM-3L, Japan Mitsui Mining Co., Ltd.), and then mix and disperse for 30 minutes at a line speed of 60m / s to obtain a thermally conductive filler with a composite structure after high-speed dispersion;
[0039]Step 2, put the thermally conductive filler of the composite structure obtained in step 1 and 20 parts of carbon fiber (length: 200 μm, diameter: 10 μm) in a vacuum mixer, and vacuumize and stir at room temperature for 30 minutes, and wait for the system to After the air is removed, stop the vacuum treatment;
[0040] Step 3, 25 parts of vinyl polyorganosiloxane (viscosity of 5000CP), 5 parts of terminal hydrogen-containing silicone oil (viscosity of 100CP, hydrogen content of 1%), 1 part of dodecyl...
Embodiment 2
[0043] Step 1, 80 parts of organosilicon microspheres (average particle diameter is 30 μm), 15 parts of organosilicon microspheres (average particle diameter is 5 μm) and 10 parts of modified nano-graphene (average particle diameter is 200nm) are added to the high-speed In the mixer (FM-3L, Mitsui Mining Co., Ltd. of Japan), then carry out mixing and dispersing for 30min at a linear speed of 60m / s to obtain a thermally conductive filler with a composite structure after high-speed dispersion;
[0044] Step 2, put the thermally conductive filler of the composite structure obtained in step 1 and 20 parts of carbon fiber (length: 200 μm, diameter: 10 μm) in a vacuum mixer, and vacuumize and stir at room temperature for 30 minutes, and wait for the system to After the air is removed, stop the vacuum treatment;
[0045] Step 3, 20 parts of vinyl polyorganosiloxane (viscosity of 3000CP), 5 parts of terminal hydrogen-containing silicone oil (viscosity of 50CP, hydrogen content of 1.5%...
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Abstract
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