Physical sorting and recycling method for positive and negative electrode materials of waste ternary lithium battery
A technology for ternary lithium batteries and positive and negative electrodes, which is applied in the field of physical separation and recovery of positive and negative electrode materials of waste ternary lithium batteries, can solve the problems of unrecovered graphite materials and high cost of chemical separation and disposal, and achieve increased floatability Sexual difference, elimination of adhesion, and high-efficiency separation
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Embodiment 1
[0027] The physical separation and recovery method of positive and negative electrode materials of waste ternary lithium batteries in this embodiment, the process flow chart is shown in figure 1 shown. The positive and negative electrode materials of a ternary lithium battery in Foshan, Guangdong were sorted according to the following steps:
[0028] (1) Put the mixed powder of positive and negative electrodes of the waste ternary lithium battery in a pyrolysis furnace, heat it for 2.0 h at a temperature of 350° C. under an inert atmosphere, and condense and collect the pyrolyzed electrode powder.
[0029] (2) Add water to the pyrolyzed electrode powder in step (1) to form a slurry with a concentration of 68% by mass and place it in a scrubbing machine for 18 minutes.
[0030] (3) Introduce the slurry after scrubbing in the step (2) into the mixing tank, add water and adjust it into a slurry with a mass percentage concentration of 12%, add water glass regulator, sodium hexame...
Embodiment 2
[0034] The physical separation and recovery method of positive and negative electrode materials of waste ternary lithium batteries in this embodiment, the process flow chart is shown in figure 1 shown. The positive and negative electrode materials of a ternary lithium battery in Shenzhen, Guangdong were sorted according to the following steps:
[0035] (1) Put the mixed positive and negative electrode powders of waste ternary lithium batteries in a pyrolysis furnace, heat them for 1.5 hours at a temperature of 400° C. under an inert atmosphere, and condense and collect them to obtain pyrolyzed electrode powders.
[0036] (2) Add water to the pyrolyzed electrode powder to form a slurry with a concentration of 70% by mass and place it in a scrubbing machine for 20 minutes.
[0037] (3) The slurry after scrubbing is introduced in the mixing tank, and water is added to be formulated into a slurry with a mass percentage concentration of 10%, and sodium carbonate regulator, sodium ...
Embodiment 3
[0041] The physical separation and recovery method of positive and negative electrode materials of waste ternary lithium batteries in this embodiment, the process flow chart is shown in figure 1 shown. The positive and negative electrode materials of a ternary lithium battery in Jiangmen, Guangdong were sorted according to the following steps:
[0042] (1) Put the positive and negative electrode mixed powder of the waste ternary lithium battery in a pyrolysis furnace, heat for 2.0 h at a temperature of 450° C. under an inert atmosphere, and condense and collect the pyrolyzed electrode powder.
[0043] (2) Add water to the pyrolyzed electrode powder to form a slurry with a concentration of 65% by mass and place it in a scrubbing machine for 15 minutes.
[0044] (3) Introduce the slurry after scrubbing in the mixing tank, add water and adjust it into a slurry with a mass percentage concentration of 15%, add sodium carbonate and water glass mixing regulator, sodium hexametaphosp...
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