Composite nanofiber membrane as well as preparation method and application thereof
A technology of composite nanofibers and fiber membranes, used in textiles, papermaking, non-woven fabrics, etc., can solve the problems of fiber discontinuity, unpredictable results, spinning breakage, etc., and achieve uniform fiber diameter distribution, good mechanical properties, and operation. simple effect
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Embodiment 1
[0034] Embodiment 1 proposes that a kind of fiber diameter is 50nm-100nm composite nanofiber film, and its preparation method comprises the following steps:
[0035] (1) Dissolving β-cyclodextrin, chitosan and gelatin in the first solvent to obtain a mixed solution with a mass concentration of 2%. Wherein, the mass ratio of the β-cyclodextrin, the chitosan and the gelatin is 1:5:0.1. The first solvent is a solvent obtained by mixing glacial acetic acid with a mass concentration of 3% and dilute hydrochloric acid with a mass concentration of 1% at a volume ratio of 1:6.
[0036] (2) Mix polyvinyl alcohol and nano-silver antibacterial agent in the second solvent to obtain a dispersion solution with a mass concentration of 1%. Wherein, the mass ratio of the polyvinyl alcohol to the nano-silver antibacterial agent is 40:1. The second solvent is a solvent obtained by mixing glycerin and 3% ethanol at a volume ratio of 1:1.
[0037] (3) The mixed solution and the dispersed soluti...
Embodiment 2
[0040] Embodiment 2 proposes that a kind of fiber diameter is 100nm-200nm composite nanofibrous film, and its preparation method comprises the following steps:
[0041] (1) Dissolving β-cyclodextrin, chitosan and gelatin in the first solvent to obtain a mixed solution with a mass concentration of 25%. Wherein, the mass ratio of the β-cyclodextrin, the chitosan and the gelatin is 1:2:3. The first solvent is a solvent obtained by mixing glacial acetic acid with a mass concentration of 1% and dilute hydrochloric acid with a mass concentration of 5% at a volume ratio of 1:2.
[0042] (2) Mix polyvinyl alcohol and nano-silver antibacterial agent in the second solvent to obtain a dispersion solution with a mass concentration of 12%. Wherein, the mass ratio of the polyvinyl alcohol to the nano-silver antibacterial agent is 20:1. The second solvent is a solvent obtained by mixing glycerin and 5% ethanol at a volume ratio of 1:3.
[0043] (3) Mix the mixed solution with the disperse...
Embodiment 3
[0046] Embodiment 3 proposes that a kind of fiber diameter is 150nm-250nm composite nanofiber film, and its preparation method comprises the following steps:
[0047](1) Dissolving β-cyclodextrin, chitosan and gelatin in the first solvent to obtain a mixed solution with a mass concentration of 12%. Wherein, the mass ratio of the β-cyclodextrin, the chitosan and the gelatin is 1:3:1. The first solvent is a solvent obtained by mixing glacial acetic acid with a mass concentration of 2% and dilute hydrochloric acid with a mass concentration of 3% at a volume ratio of 1:4.
[0048] (2) Mix polyvinyl alcohol and nano-silver antibacterial agent in the second solvent to obtain a dispersion solution with a mass concentration of 6%. Wherein, the mass ratio of the polyvinyl alcohol to the nano-silver antibacterial agent is 30:1. The second solvent is a solvent obtained by mixing glycerin and ethanol with a concentration not greater than 5% at a volume ratio of 1:2.
[0049] (3) Mix th...
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