A method of modifying mc nylon with flexible hydrogenated c9 petroleum resin
A petroleum resin and flexible technology, applied in the field of polymer material modification, can solve the problems of decreased tensile strength of materials, low impact strength at low temperature, limited application scope, etc., to improve tensile strength, reduce production costs, and broaden application fields Effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0024] Weigh the following components by mass percentage: 28% maleic anhydride, 69% n-octadecanol, 1.5% toluenesulfonic acid, 1.5% petroleum ether, and add them to a four-necked bottle with a stirring device in turn. A reflux condenser and a water separator are installed on the bottle, and then heated to 120 ℃ with an electric heating insulation jacket to carry out the esterification reaction. The water generated by the reaction and the water-carrying agent form an azeotrope and are distilled out, and the water is separated by a water separator. When the amount of water is equal to the theoretical water output or the water output is no longer increased, the esterification reaction is completed. ;
[0025] 100g C9 petroleum resin was put into the four-necked bottle with stirring device, and the oil bath was heated to a molten state, and 10g of the above-obtained di-n-stearyl maleate was added, and 1.5g of di-n-stearyl maleate was added in batches at 200° C. Azobisisobutyronitr...
Embodiment 2
[0029] Weigh the following components by mass percentage: 18% maleic anhydride, 80% n-heptanol, 0.5% toluenesulfonic acid, 1.5% toluene, and add them to a four-necked bottle with a stirring device in turn, and put them on the four-necked bottle. The reflux condenser and the water separator are then heated to 100 ℃ with an electric heating insulation jacket to carry out the esterification reaction. The water generated by the reaction and the water-carrying agent form an azeotrope and are distilled out, and the water is separated by a water separator. When it is equal to the theoretical water output or the water output is no longer increased, the esterification reaction is completed, and the product is subjected to vacuum distillation, alkali washing, water washing and vacuum drying to obtain milky white waxy n-heptanol maleate;
[0030] 100g C9 petroleum resin is put into the four-necked flask with stirring device, and the oil bath is heated to a molten state, and 5g of the abov...
Embodiment 3
[0034] Weigh the following components by mass percentage: 28% maleic anhydride, 69% n-pentacosanol, 1.5% toluenesulfonic acid, 1.5% cyclohexane, and add them to a four-necked flask with a stirring device in turn. The four-necked bottle is equipped with a reflux condenser and a water separator, and then heated to 120°C with an electric heating jacket to carry out the esterification reaction. The water generated by the reaction and the water-carrying agent form an azeotrope and steam out, and the water is separated by a water separator. When the amount of water removed from the system is equal to the theoretical water output or the water output no longer increases, the esterification reaction is completed. pentadecanol ester;
[0035] 100g C9 petroleum resin is put into the four-necked bottle with stirring device, the oil bath is heated to the molten state, 15g of the above-obtained bis-n-pentacosyl maleate is added, and azo is added in batches at 180° C. Dimethyl diisobutyrate...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More