Two-component high-thermal-conductivity self-leveling pouring sealant as well as preparation method and application thereof
A high thermal conductivity, self-leveling technology, used in adhesives, polymer adhesive additives, non-polymer adhesive additives, etc. Problems such as poor flatness
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Embodiment 1
[0041] A two-component high thermal conductivity self-leveling potting glue, including A component and B component prepared by the following steps; when the two-component high thermal conductivity self-leveling potting glue is used, the A component and the B component According to the mass ratio of 1:1 mixed evenly obtained. The parts are all parts by mass.
[0042] (1) Preparation of component A: Vinyl-terminated silicone oil (vinyl-terminated poly(dimethylsiloxane), 100mPa.s, vinyl mass content 1.06±0.03%, model RH-Vi100E, Zhejiang Runhe Organic Silicon New Materials Co., Ltd.) 6.5 parts, surface treatment agent cyclohexylmethyldimethoxysilane 0.2 parts were added to the power mixer in turn, the dispersion frequency was 10Hz, the revolution frequency was 20Hz, stirred for 10 minutes, and then the heat-conducting filler was spherically formed in batches Alumina mixture (50 parts with a median particle size of 80 μm, 30 parts with a median particle size of 12 μm, and 13 parts...
Embodiment 2
[0045] A two-component high thermal conductivity self-leveling potting glue, including A component and B component prepared by the following steps; when the two-component high thermal conductivity self-leveling potting glue is used, the A component and the B component According to the mass ratio of 1:1 mixed evenly obtained. The parts are all parts by mass.
[0046] (1) Preparation of component A: 6.5 parts of vinyl-terminated silicone oil (50mPa.s, vinyl mass content 2.0%, model RH-Vi50E, Zhejiang Runhe Silicone New Material Co., Ltd.), surface treatment agent phenylmethyl Add 0.2 parts of dimethoxysilane into the power mixer in turn, stir at a dispersion frequency of 10 Hz and a revolution frequency of 20 Hz for 10 minutes, and then add thermally conductive filler spherical alumina mixture (40 parts with a median particle size of 60 μm, and 30 parts with a median particle size of 8 μm) in batches. Parts, median particle size 0.5μm (23 parts) 93 parts, black material (carbon...
Embodiment 3
[0049] A two-component high thermal conductivity self-leveling potting glue, including A component and B component prepared by the following steps; when the two-component high thermal conductivity self-leveling potting glue is used, the A component and the B component According to the mass ratio of 1:1 mixed evenly obtained. The parts are all parts by mass.
[0050] (1) Preparation of component A: 6.5 parts of vinyl-terminated silicone oil (70mPa.s, vinyl mass content 1.45±0.15%, model RH-Vi70E, Zhejiang Runhe Silicone New Material Co., Ltd.), surface treatment agent ring Add 0.1 part of hexylmethyldimethoxysilane and 0.1 part of phenylmethyldimethoxysilane into the power mixer in turn, stir for 10 minutes at a dispersion frequency of 10 Hz and a revolution frequency of 20 Hz, and then add thermally conductive filler spherical alumina in batches Mixture (45 parts with a median particle size of 70 μm, 30 parts with a median particle size of 10 μm, and 18 parts with a median pa...
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