Low-energy cured photoresist, and resist pattern and preparation method thereof
A resist pattern and photoresist technology, applied in the photoresist field, can solve the problems of slow curing rate of photocurable resin, reduced photoresist resolution, low photoresist gel rate, etc., and achieves easy scale. Production, excellent resolution, wide range of absorption spectrum effects
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preparation example 1
[0044] Preparation Example 1: Preparation of A with a molecular weight of 88w
[0045] S1, weigh methpropionate, methyl methacrylate, and butyl acrylate, and put them into the reactor according to the mass ratio of 22:71:7;
[0046] S2, feed N into the reactor 2 , Add manganese dioxide into the reactor with a weight ratio of butyl acrylate: manganese dioxide of 10:1, control the temperature at 56°C, and react at 50r / min for 5h to obtain A.
preparation example 2
[0047] Preparation Example 2: Preparation of A with a molecular weight of 100w
[0048] S1, weigh methpropionate, methyl methacrylate, and butyl acrylate, and put them into the reactor according to the mass ratio of 22:71:7;
[0049] S2, feed N into the reactor 2 , Add manganese dioxide into the reactor with butyl acrylate: manganese dioxide weight ratio of 7:1, control the temperature at 62°C, and react at 50r / min for 6h to obtain A.
preparation example 3
[0050] Preparation example 3: the preparation of A with a molecular weight of 109w
[0051] S1, weigh methpropionate, methyl methacrylate, and butyl acrylate, and put them into the reactor according to the mass ratio of 22:71:7;
[0052] S2, feed N into the reactor 2 , Add manganese dioxide into the reactor with butyl acrylate: manganese dioxide weight ratio of 5:1, control the temperature at 65°C, react at 50r / min for 7h, and obtain A.
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