A preparation method of modified carbon nanotube reinforced aluminum alloy semi-solid slurry
A technology of semi-solid slurry and carbon nanotubes, which is applied in the field of metal material manufacturing, can solve the problems of easy growth of material grains, easy agglomeration of carbon nanotubes, and poor bonding of melt interfaces, so as to achieve uniform distribution of reinforcing phases and improve The effect of improving bonding quality and bonding strength
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Embodiment 1
[0041] A preparation method of modified carbon nanotube reinforced aluminum alloy semi-solid slurry:
[0042] (1) Take an Al-Si alloy, the proportion of each element in the alloy is: Si 6.95%-7.15%, Mg 0.30%-0.35%, and the balance is Al; prepare carbon nanotubes: the outer diameter is 20-60nm, and the length is 10-30μm, purity ≥99.9%; aluminum powder: purity ≥99.9%, particle size 100-200 mesh.
[0043] (2) Prepare an acid solution with a volume ratio of concentrated nitric acid and concentrated sulfuric acid of 1:3, add 3.0 g of carbon nanotubes per 100 mL of acid solution, heat to 80 ° C under magnetic stirring, condense and reflux for 4 hours, and the magnetic stirring speed The temperature is 900r / min, and then filtered with deionized water for 3-4 times until the filtrate is neutral, then placed in a vacuum drying oven to raise the temperature to 70°C, and kept for 18 hours to obtain purified carbon nanotubes.
[0044] (3) ① With zirconium oxychloride as the source of zir...
Embodiment 2
[0049] A preparation method of modified carbon nanotube reinforced aluminum alloy semi-solid slurry:
[0050] (1) Take an Al-Si alloy, the proportion of each element in the alloy is: Si 6.95%-7.15%, Mg 0.30%-0.35%, and the balance is Al; prepare carbon nanotubes: the outer diameter is 20-60nm, and the length is 10-30μm, purity ≥99.9%; aluminum powder: purity ≥99.9%, particle size 100-200 mesh.
[0051] (2) Prepare an acid solution with a volume ratio of concentrated nitric acid and concentrated sulfuric acid of 1:2.5, add 2.5 g of carbon nanotubes per 100 mL of acid solution, heat to 80 ° C under magnetic stirring, condense and reflux for 4 hours, and the magnetic stirring speed 800r / min, and then filter with deionized water for 3-4 times until the filtrate is neutral, then place it in a vacuum drying oven to raise the temperature to 70°C, and keep it warm for 15 hours to obtain purified carbon nanotubes.
[0052] (3) ① With zirconium oxychloride as the source of zirconium, a...
Embodiment 3
[0057] A preparation method of modified carbon nanotube reinforced aluminum alloy semi-solid slurry:
[0058] (1) Take an Al-Si alloy, the proportion of each element in the alloy is: Si 6.95%-7.15%, Mg 0.30%-0.35%, and the balance is Al; prepare carbon nanotubes: the outer diameter is 20-60nm, and the length is 10-30μm, purity ≥99.9%; aluminum powder: purity ≥99.9%, particle size 100-200 mesh.
[0059] (2) Prepare an acid solution with a volume ratio of concentrated nitric acid and concentrated sulfuric acid of 1:3.5, add 3.5 g of carbon nanotubes for every 100 mL of acid solution, heat to 80 ° C under magnetic stirring, condense and reflux for 4 hours, and the magnetic stirring speed The temperature is 1000r / min, and then filtered with deionized water for 3-4 times until the filtrate is neutral, then placed in a vacuum drying oven and heated to 70°C, and kept for 20 hours to obtain purified carbon nanotubes.
[0060] (3) ① With zirconium oxychloride as the source of zirconiu...
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