Drought-resistant soil-loosening auxiliary agent containing polyglutamic acid
A technology of polyglutamic acid and polyglutamic acid master, which is applied in the field of drought-resistant soil loosening additives, can solve the problems of restricting wide application, short duration, high cost, etc., and achieve low pollution-free cost, simple production process, Fast and dramatic results
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Embodiment 1
[0014] 1) Take 20g of starch and 180g of deionized water and add them to a four-necked flask equipped with a stirrer, thermometer, reflux condenser and nitrogen air pipe, stir evenly, place the reaction bottle in a constant temperature water bath, gelatinize at 80°C for 20min, and cool to 40°C.
[0015] 2) Add 120 g of acrylic acid (AA) partially neutralized with NaOH solution, 0.2 g of cross-linking agent N,N-nitrosobisacrylamide, and 210 g of yeast fermentation waste liquid to form a dispersion solution with gelatinized starch. Nitrogen was introduced to protect it for 10 minutes, 0.1 g of ammonium persulfate was added to initiate the reaction for 15 minutes, and the temperature was kept to stir for 4 hours.
[0016] 3) dividing the material obtained in step 2) into small pieces, and drying in an oven at 70° C.;
[0017] 4) Pulverize the dried material and take 0.01-1.0mm particles to obtain the drought-resistant soil loosening agent containing polyglutamic acid.
[0018] ...
Embodiment 2
[0020] 1) Take 23g of starch and 207g of deionized water and add them to a four-necked flask equipped with a stirrer, thermometer, reflux condenser and nitrogen air duct, stir evenly, place the reaction bottle in a constant temperature water bath, gelatinize at 80°C for 20min, and cool to 40°C.
[0021] 2) Add 135g of acrylic acid (AA) partially neutralized with NaOH solution, 0.25g of cross-linking agent N,N-nitrosobisacrylamide, and 240g of yeast fermentation waste liquid to form a dispersion solution with gelatinized starch. Nitrogen was introduced to protect it for 10 minutes, 0.1 g of ammonium persulfate was added to initiate the reaction for 15 minutes, and the temperature was kept to stir for 4 hours.
[0022] 3) dividing the material obtained in step 2) into small pieces, and drying in an oven at 70° C.;
[0023] 4) Pulverize the dried material and take 0.01-1.0mm particles to obtain the drought-resistant soil loosening agent containing polyglutamic acid.
[0024] Th...
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