Nanometer composite material for absorbing near-infrared light
A near-infrared light and composite material technology, applied in the field of polymer materials, can solve problems such as the darkening of LCD TV screen, and achieve the effect of remarkable effect and good use prospect.
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Embodiment 1
[0037] Weigh 0.25g of CdO and add it into a 50ml three-neck flask. Then weigh 2.5ml of oleic acid and 2.5ml of octadecene solvent with a graduated cylinder and place them in a three-necked flask. Place the three-necked flask on a constant temperature magnetic stirrer to ensure that it is under N 2 The temperature was raised to 250°C at a constant rate under ambient conditions. The solution in the flask became clear and yellowish. The temperature was lowered to room temperature, and it was reserved for the next experiment.
[0038] Take 0.04g of Se powder with a weighing balance, accurately pipette 0.5ml and place it in a test tube. The mixture was ultrasonically dissolved in a sonicator, and the solution in the test tube became clear, which was reserved for the next experiment.
[0039] Mix 0.3ml of tri-n-octylphosphorus solution, 0.2ml of the solution obtained in step a and 5ml of oleylamine in a 50ml three-necked flask, and place the reaction system under N 2 The temper...
Embodiment 2
[0042] Weigh 0.25g of CdO and add it into a 50ml three-neck flask. Then weigh 2.5ml of oleic acid and 2.5ml of octadecene solvent with a graduated cylinder and place them in a three-necked flask. Place the three-necked flask on a constant temperature magnetic stirrer to ensure that it is under N 2 The temperature was raised to 250°C at a constant rate under ambient conditions. The solution in the flask became clear and yellowish. The temperature was lowered to room temperature, and it was reserved for the next experiment.
[0043] Take 0.04g of Se powder with a weighing balance, accurately pipette 0.5ml and place it in a test tube. The mixture was ultrasonically dissolved in a sonicator, and the solution in the test tube became clear, which was reserved for the next experiment.
[0044] Mix 0.3ml of tri-n-octylphosphorus solution, 0.2ml of the solution obtained in step a and 5ml of oleylamine in a 50ml three-necked flask, and place the reaction system under N 2 The temperat...
Embodiment 3
[0047] Weigh 0.12gCuCl 2 Add 50ml of the mountain mouth flask, and then weigh 2ml of oleic acid and 2ml of ethylene glycol reagent with a measuring cylinder and place them in the three-necked flask. Adjust the pH value to 4 with concentrated hydrochloric acid to ensure that the three-necked flask is under N 2 environment to react. The solution in the flask became clear and yellowish. The temperature was lowered to room temperature, and it was reserved for the next experiment.
[0048] Take 0.04g EuCl with a weighing balance 2 , Accurately pipette 0.5ml into a test tube. The mixture was ultrasonically dissolved in a sonicator, and the solution in the test tube became clear, which was reserved for the next experiment.
[0049] Mix 0.3ml of tri-n-octylphosphorus solution, 0.2ml of the solution obtained in step a and 5ml of oleylamine in a 50ml three-necked flask, and place the reaction system under N 2 The temperature was raised to 275°C at a constant rate under ambient con...
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