Multi-component epoxy sealing silica gel and preparation method thereof
An epoxy sealing, multi-component technology, applied in the direction of epoxy resin glue, adhesive, adhesive type, etc., can solve the problems of flammable foam, non-environmental protection, waste and other problems
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[0115] 1) Preparation of component A: first fully mix the epoxy resin and reactive diluent, then add inorganic fillers and continue mixing evenly to obtain component A.
[0116] 2) Preparation of component B: first knead vinyl silicone oil and white carbon black, then add platinum catalyst, tungsten nitride, antistatic agent and continue kneading evenly to obtain component B.
[0117] 3) Preparation of component C: Knead vinyl silicone oil, hydrogen-containing silicone oil and white carbon black first. Then add MQ resin and curing agent to continue kneading. Finally, add the inhibitor and knead evenly to obtain component C.
[0118] 4) Preparation of multi-component epoxy sealing silica gel: Mix components A, B and C in proportion to obtain epoxy sealing silica gel.
Embodiment 1
[0120] Stir and mix 72 parts of epoxy resin and 5 parts of reactive diluent at 70°C. After 25 minutes, turn on high-speed stirring and vacuumize to -0.03MPa. The high-speed stirring time is 35 minutes. Then add 23 parts of inorganic fillers and continue stirring for 25 minutes, cool down and stop stirring, stop stirring for 10 minutes and stop vacuuming to obtain component A.
[0121] Add 64 parts of terminal vinyl silicone oil and 8 parts of polyvinyl silicone oil into the kneader, then add 20 parts of hydrophobic fumed silica in 5 times, and continue kneading for 1 hour after the kneader finishes eating the powder. Finally, add 0.4 parts of platinum catalyst, 3.8 parts of tungsten nitride fiber and 3.8 parts of antistatic agent and continue kneading for 20 minutes to obtain component B.
[0122] Add 42.5 parts of terminal vinyl silicone oil, 5.5 parts of polyvinyl silicone oil and 9 parts of hydrogen-containing silicone oil into the kneader, then add 13 parts of hydrophobic ...
Embodiment 2
[0125] Stir and mix 72 parts of epoxy resin and 5 parts of reactive diluent at 70°C. After 25 minutes, turn on high-speed stirring and vacuumize to -0.03MPa. The high-speed stirring time is 35 minutes. Then add 23 parts of inorganic fillers and continue stirring for 25 minutes, cool down and stop stirring, stop stirring for 10 minutes and stop vacuuming to obtain component A.
[0126] Add 50 parts of terminal vinyl silicone oil and 24 parts of polyvinyl silicone oil into the kneader, then add 18 parts of hydrophobic fumed silica in 5 times, and continue kneading for 1 hour after the kneader finishes eating the powder. Finally, add 0.4 parts of platinum catalyst, 3.5 parts of tungsten nitride fiber and 4.1 parts of antistatic agent and continue kneading for 20 minutes to obtain component B.
[0127] Add 30 parts of terminal vinyl silicone oil, 18 parts of polyvinyl silicone oil and 8 parts of hydrogen-containing silicone oil into the kneader, then add 12 parts of hydrophobic fu...
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