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Detection method of foundation-consolidating and life-prolonging pill

A detection method and a trillium technology, which can be used in measurement devices, instruments, scientific instruments, etc., to solve the problems of difficulty in detection and verification, inability to achieve treatment, and human toxicity.

Pending Publication Date: 2021-11-12
JIANGXI UNIVERSE PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It contains a variety of valuable medicinal materials, such as Salvia miltiorrhiza, Cistanche, ginseng, etc. However, in recent years, in order to earn illegal profits, some unscrupulous merchants have not added valuable Chinese medicinal materials such as Salvia miltiorrhiza, Cistanche, and ginseng in the preparation process of Guben Trillium Pills. Do not add a few Chinese herbal medicines in the prescription to achieve the purpose of reducing production costs. Products without Chinese herbal medicines will not only fail to achieve the purpose of treatment, but even cannot be compatible with the whole prescription because of the lack of a single medicine, which will be poisonous to the human body effect
However, as far as the current situation is concerned, the identification of the authenticity of the drug is only through the label on the product packaging, and there is no strict method for testing it in the laboratory. This is a serious defect in the detection of drugs. In view of the above problems, this The invention provides a laboratory detection method for Guben Trillium Pills. Through the test method provided by the invention, it can be detected and identified whether the drug is Guben Trillium Pills, and whether there are few medicinal materials added in the product, because Guben Trillium Pills The complexity of the formula has brought great difficulties to the detection and verification work, so the present invention provides a characteristic detection method of Guben Trillium Pills, which improves the detection efficiency while ensuring the detection accuracy

Method used

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  • Detection method of foundation-consolidating and life-prolonging pill
  • Detection method of foundation-consolidating and life-prolonging pill

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0053] A kind of detection method of consolidating trillium pill, concrete detection method comprises:

[0054] 1) Preparation method of standard identification solution:

[0055] 1) Take 12g of Salvia miltiorrhiza, wash it, put it into ethanol solution, heat to 110°C, turn on the condensing reflux device while heating, and boil for 22 minutes; collect the ethanol solution by filtration, add anhydrous magnesium sulfate to the ethanol solution to absorb the Moisture, filter again to collect the filtrate, evaporate the filtrate through a rotary evaporator to obtain a residue, add petroleum ether to the residue until it is completely dissolved, and obtain the Salvia miltiorrhiza identification solution;

[0056] 2) Take 12g of Cistanche, add butanol solution to it, heat it, raise the temperature to 50°C and keep the solution warm, ultrasonically treat the warm solution for 30min, then filter it, collect the filtrate and filter residue, and filter the filter residue again Perform...

Embodiment 2

[0095] A kind of detection method of consolidating trillium pill, concrete detection method comprises:

[0096] 1) Preparation method of standard identification solution:

[0097] 1) Take 12g of Salvia miltiorrhiza, wash it, put it into ethanol solution, heat to 110°C, turn on the condensing reflux device while heating, and boil for 22 minutes; collect the ethanol solution by filtration, add anhydrous magnesium sulfate to the ethanol solution to absorb the Moisture, filter again to collect the filtrate, evaporate the filtrate through a rotary evaporator to obtain a residue, add petroleum ether to the residue until it is completely dissolved, and obtain the Salvia miltiorrhiza identification solution;

[0098] 2) Take 12g of Cistanche, add butanol solution to it, heat it, raise the temperature to 50°C and keep the solution warm, ultrasonically treat the warm solution for 30min, then filter it, collect the filtrate and filter residue, and filter the filter residue again Perform...

Embodiment 3

[0137] A kind of detection method of consolidating trillium pill, concrete detection method comprises:

[0138] 1) Preparation method of standard identification solution:

[0139] 1) Take 12g of Salvia miltiorrhiza, wash it, put it into ethanol solution, heat to 110°C, turn on the condensing reflux device while heating, and boil for 22 minutes; collect the ethanol solution by filtration, add anhydrous magnesium sulfate to the ethanol solution to absorb the Moisture, filter again to collect the filtrate, evaporate the filtrate through a rotary evaporator to obtain a residue, add petroleum ether to the residue until it is completely dissolved, and obtain the Salvia miltiorrhiza identification solution;

[0140] 2) Take 12g of Cistanche, add butanol solution to it, heat it, raise the temperature to 50°C and keep the solution warm, ultrasonically treat the warm solution for 30min, then filter it, collect the filtrate and filter residue, and filter the filter residue again Perform...

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Abstract

The invention provides a detection method of a foundation strengthening and life prolonging pill. Effective components in the foundation-consolidating and life-prolonging pill are extracted, and an extracting agent and a drying agent are added into the foundation-consolidating and life-prolonging pill, so that the extraction rate of the effective components is increased, and preparation is made for subsequent detection; during detection, whether corresponding components exist in the foundation-consolidating and life-prolonging pill or not is compared and verified by preparing a medicinal material identification solution. Salvia miltiorrhiza, cistanche and semen cuscutae are selected as main identification indexes of the foundation-consolidating and life-prolonging pill, and ginseng, radix ophiopogonis, schisandra chinensis, asparagus cochinchinensis and prepared rehmannia root are selected as auxiliary identification methods of the foundation-consolidating and life-prolonging pill. The identification of all components is avoided, the detection process is simplified, the detection time is shortened, and meanwhile, the detection accuracy cannot be reduced. The antioxidant color reducer protects the effective components from being oxidized, weakens the color of the solution and reduces the detection difficulty.

Description

technical field [0001] The invention relates to the technical field of drug quality control, in particular to a detection method for Guben Trillium Pills. Background technique [0002] Guben Trillium Pills, also known as Bainian Dan, is a national medicine standard drug. It has been certified by the State Food and Drug Administration. It is used for fatigue and injury, low back pain and body fatigue, palpitation, insomnia, haggard skin, premature graying of beard and hair, irregular menstrual blood, loss of appetite, senile dementia, sexual aging, high blood pressure, diabetes, menopausal syndrome, etc. It contains a variety of valuable medicinal materials, such as Salvia miltiorrhiza, Cistanche, ginseng, etc. However, in recent years, in order to earn illegal profits, some unscrupulous merchants have not added valuable Chinese medicinal materials such as Salvia miltiorrhiza, Cistanche, and ginseng in the preparation process of Guben Trillium Pills. Do not add a few Chinese...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/90G01N30/91G01N30/94G01N30/95
CPCG01N30/90G01N30/94G01N30/95G01N30/91Y02A50/30
Inventor 眭荣春胡庭国肖云王志春
Owner JIANGXI UNIVERSE PHARMA
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