Bactericidal composition containing captan and cymoxanil and preparation method thereof
The technology of a composition and captan, which is applied in the field of fungicide preparation, can solve the problems of mediocre bactericidal effect, affected crop harvest, long effective time, etc.
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Embodiment 1
[0033] A bactericidal composition containing captan and cymoxanil, the bactericidal composition includes the following raw materials in parts by weight: 1 part of captan, 90 parts of cyanazazole, 20 parts of bactericidal enhancer, and the balance is auxiliary components;
[0034] The preparation method of this pesticide composition specifically comprises the steps:
[0035] The above raw materials are weighed, mixed evenly, and according to the dosage form, a bactericidal composition suspension is prepared.
[0036] Wherein, the bactericidal enhancer is made by the following steps:
[0037] Step A1: Mix 2-chloro-4-nitrophenylacetic acid, copper chloride, and sodium hydroxide aqueous solution evenly, then stir and reflux for 5 hours under the conditions of rotating speed of 150r / min and temperature of 160°C to obtain intermediate Body 1, mix intermediate 1, toluene, and p-toluenesulfonic acid evenly, at a temperature of 120°C, reflux for 3 hours, then add aluminum trichloride ...
Embodiment 2
[0042] A bactericidal composition containing captan and cymoxanil, the bactericidal composition includes the following raw materials in parts by weight: 45 parts of captan, 45 parts of cyanazazole, 23 parts of bactericidal enhancer, and the balance is auxiliary components;
[0043] The preparation method of this pesticide composition specifically comprises the steps:
[0044] The above raw materials are weighed, mixed evenly, and according to the dosage form, water-dispersible granules of the fungicidal composition are obtained.
[0045] Wherein, the bactericidal enhancer is made by the following steps:
[0046] Step A1: Mix 2-chloro-4-nitrophenylacetic acid, copper chloride, and sodium hydroxide aqueous solution evenly, then stir and reflux for 6 hours under the conditions of rotation speed of 180r / min and temperature of 170°C to obtain intermediate Body 1, mix intermediate 1, toluene, and p-toluenesulfonic acid evenly, and react under reflux for 4 hours at a temperature of ...
Embodiment 3
[0051] A bactericidal composition containing captan and cymoxanil, the bactericidal composition includes the following raw materials in parts by weight: 90 parts of captan, 1 part of cyanazazole, 25 parts of bactericidal enhancer, and the balance is auxiliary components;
[0052] The preparation method of this pesticide composition specifically comprises the steps:
[0053] The above raw materials are weighed, mixed evenly, and according to the dosage form, a wettable powder of the fungicidal composition is obtained.
[0054] Wherein, the bactericidal enhancer is made by the following steps:
[0055] Step A1: Mix 2-chloro-4-nitrophenylacetic acid, copper chloride, and sodium hydroxide aqueous solution evenly, then stir and reflux for 7 hours at a rotation speed of 200r / min and a temperature of 180°C to obtain intermediate Body 1, mix intermediate 1, toluene, and p-toluenesulfonic acid evenly, at a temperature of 130°C, reflux for 5 hours, then add aluminum trichloride and tri...
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