Method for treating aramid fiber doped modified cellulose insulation paper by plasma

A plasma and aramid fiber technology, which is applied in the fields of synthetic cellulose/non-cellulose material pulp/paper, fiber raw material processing, papermaking, etc., can solve the problem of poor interface binding ability between aramid fiber 1313 and natural cellulose, composite insulating paper Low mechanical properties, uneven distribution of electric field, etc., to achieve the effect of increasing breakdown field strength and discharge initiation voltage, improving interface incompatibility, and improving uneven distribution of electric field

Active Publication Date: 2021-12-14
CHONGQING UNIV
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Problems solved by technology

[0007]Aiming at the above-mentioned problems existing in the prior art, the technical problem to be solved by the present invention is: the high dielectric constant of cellulose insulating paper leads to electric field distribution when used

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  • Method for treating aramid fiber doped modified cellulose insulation paper by plasma
  • Method for treating aramid fiber doped modified cellulose insulation paper by plasma
  • Method for treating aramid fiber doped modified cellulose insulation paper by plasma

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Embodiment Construction

[0044] The present invention will be described in further detail below.

[0045] Doping different contents of aramid 1313 (PMTA) chopped fibers in natural cellulose pulp can reduce the dielectric constant and dielectric loss of insulating paper, but due to the poor bonding ability of the two fibers, the composite insulating paper sample mechanically Performance is drastically reduced. In order to make up for this defect, the present invention expounds the improvement effect of low-temperature plasma treatment on the binding ability of two kinds of cellulose, and tests and analyzes the properties of the prepared composite insulating paper. The results show that low-temperature plasma treatment can effectively improve the two kinds of cellulose The binding force between the fibers can make up for the loss of mechanical properties, but has little effect on the dielectric and breakdown properties of insulating paper. Insulating paper samples prepared by doping 10% PMTA in natural...

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Abstract

The invention relates to a method for treating aramid fiber doped modified cellulose insulation paper through plasma. The method comprises the following steps: firstly, soaking PMTA chopped fibers in a solution capable of removing attachments for a long time, and then taking out and washing the PMTA chopped fibers; putting the clean short fibers into a vacuum oven at 100 DEG C, drying for a plurality of hours, and putting into a low-temperature plasma reaction cavity; pumping the sealing cavity to low pressure, introducing NH3 gas, vacuumizing, and repeating the steps for multiple times; introducing NH3 into a vacuum sealing cavity, and keeping the constant atmospheric pressure in the cavity ; and under the constant atmospheric pressure, keeping stable high-frequency power supply voltage for continuous treatment for a period of time, and introducing nitrogen until the atmospheric pressure is the same as the external atmospheric pressure after the treatment is finished, so as to obtain the prepared PMTA chopped fiber. According to the aramid fiber modified by the low-temperature plasma, the binding force between the aramid fiber and a base material is improved, no pollution is caused during preparation, no catalyst is needed, more importantly, no damage is caused to the fiber, and the excellent performance of the PMTA can be kept.

Description

technical field [0001] The invention relates to the field of cellulose insulating paper, in particular to a method for plasma treating aramid fiber doped modified cellulose insulating paper. Background technique [0002] The existing composite insulation composed of insulating paper and insulating oil is the most widely used form of internal insulation for oil-immersed power equipment. Among them, natural cellulose insulating paper is widely used because of its good insulation and mechanical properties, environmental protection, renewability, and economy. In oil-paper insulation. Lignocellulose is made into insulating cardboard after papermaking processes such as beating and molding, and the dielectric constant (ε cellulose ≈4.1-4.8) is about the dielectric constant of mineral insulating oil (ε oil ≈2.2) twice or more. Under the alternating field strength, the insulating oil bears a higher field strength, and its breakdown field strength is much smaller than that of insul...

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Application Information

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IPC IPC(8): D21H13/26C08J5/06
CPCD21H13/26C08J5/06Y02W30/64
Inventor 杨丽君侯微袁媛郝建成立赵学童何雨欣冯勇
Owner CHONGQING UNIV
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